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C9H18N2

Base Information Edit
C<sub>9</sub>H<sub>18</sub>N<sub>2</sub>

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of C9H18N2 Edit
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Technology Process of C9H18N2

There total 17 articles about C9H18N2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 23 ℃; for 4h;
DOI:10.3987/COM-18-S(T)66
Guidance literature:
(1S,9aR)-octahydro-1H-quinolizine-1-carboxylic acid; With diphenyl phosphoryl azide; triethylamine; In toluene; Inert atmosphere; Reflux;
With hydrogenchloride; In water; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2011.07.017
Guidance literature:
Multi-step reaction with 10 steps
1.1: (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; benzoic acid / chloroform / 22 h / -50 °C / Inert atmosphere
2.1: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / methanol; water; acetonitrile / 3 h / 0 - 20 °C / Inert atmosphere
3.1: methanol / diethyl ether; toluene / 3 h / 0 - 20 °C / Inert atmosphere
4.1: lithium diisopropyl amide / diethyl ether / 1 h / -100 °C / Inert atmosphere
4.2: 1 h / -100 °C / Inert atmosphere
5.1: dimethylsulfide borane complex / hexane / 0 °C / Inert atmosphere
5.2: 1 h / Inert atmosphere; Reflux
6.1: triethylamine / dichloromethane / 2 h / Inert atmosphere
7.1: 1.5 h / 20 °C / Inert atmosphere
8.1: sodium hydroxide / dichloromethane; water / Inert atmosphere
9.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 4 h / 0 - 20 °C / Inert atmosphere
10.1: diphenyl phosphoryl azide; triethylamine / toluene / Inert atmosphere; Reflux
10.2: 0.5 h / Inert atmosphere
With (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; methanol; sodium chlorite; sodium dihydrogenphosphate; lithium hydroxide monohydrate; dimethylsulfide borane complex; diphenyl phosphoryl azide; dihydrogen peroxide; triethylamine; benzoic acid; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; chloroform; water; toluene; acetonitrile; 1.1: aza-Michael reaction;
DOI:10.1016/j.tet.2011.07.017
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