C₅₅H₆₀N₂O₉SSi₂

Base Information

Chemical Name:C₅₅H₆₀N₂O₉SSi₂
CAS No.:1352916-63-2
Molecular Formula:C₅₅H₆₀N₂O₉SSi₂
Molecular Weight:981.326
Hs Code.:

C<sub>55</sub>H<sub>60</sub>N<sub>2</sub>O<sub>9</sub>SSi<sub>2</sub>

Synonyms:

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Chemical Property of C₅₅H₆₀N₂O₉SSi₂

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Technology Process of C₅₅H₆₀N₂O₉SSi₂

There total 11 articles about C₅₅H₆₀N₂O₉SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10393-86-9
methanesulphonyl hydrazide

: 1352916-62-1
C₅₄H₅₆O₈Si₂

: 1352916-63-2
C₅₅H₆₀N₂O₉SSi₂

Guidance literature:: With trifluoroacetic acid; In water; isopropyl alcohol; at 20 ℃; for 62h; Inert atmosphere;
DOI:10.1002/anie.201104504

Reference yield:

: 1352916-43-8
C₃₀H₄₀O₉Si

: 1352916-63-2
C₅₅H₆₀N₂O₉SSi₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium triethylborohydride / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.1: dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

3.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 15 h / 0 °C / Inert atmosphere

4.1: pyridine; Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.1: sodium chlorite; disodium hydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 0 °C / Inert atmosphere

6.1: trifluoroacetic anhydride / nitromethane / 2.5 h / 80 °C / Inert atmosphere; Molecular sieve

6.2: 2 h / 20 °C / Inert atmosphere

7.1: 1H-imidazole; dmap / dichloromethane / 20 h / 20 °C / Inert atmosphere

8.1: trifluoroacetic acid / water; isopropyl alcohol / 62 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; sodium chlorite; disodium hydrogenphosphate; 2-methyl-but-2-ene; lithium triethylborohydride; Dess-Martin periodane; pyridine hydrogenfluoride; trifluoroacetic acid; trifluoroacetic anhydride; In tetrahydrofuran; nitromethane; dichloromethane; water; isopropyl alcohol; tert-butyl alcohol; 6.1: Friedel Crafts acylation;
DOI:10.1002/anie.201104504

Reference yield:

: 1352916-53-0
C₃₅H₅₀O₁₁Si

: 1352916-63-2
C₅₅H₆₀N₂O₉SSi₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 15 h / 0 °C / Inert atmosphere

2.1: pyridine; Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.1: sodium chlorite; disodium hydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 0 °C / Inert atmosphere

4.1: trifluoroacetic anhydride / nitromethane / 2.5 h / 80 °C / Inert atmosphere; Molecular sieve

4.2: 2 h / 20 °C / Inert atmosphere

5.1: 1H-imidazole; dmap / dichloromethane / 20 h / 20 °C / Inert atmosphere

6.1: trifluoroacetic acid / water; isopropyl alcohol / 62 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; sodium chlorite; disodium hydrogenphosphate; 2-methyl-but-2-ene; Dess-Martin periodane; pyridine hydrogenfluoride; trifluoroacetic acid; trifluoroacetic anhydride; In tetrahydrofuran; nitromethane; dichloromethane; water; isopropyl alcohol; tert-butyl alcohol; 4.1: Friedel Crafts acylation;
DOI:10.1002/anie.201104504