(2S)-2--4-methylpentan-1-ol

Base Information

• Chemical Name: (2S)-2--4-methylpentan-1-ol
• CAS No.: 111633-84-2
• Molecular Formula: C₂₃H₃₀N₂O₄
• Molecular Weight: 398.502

Synonyms:

Chemical Property of (2S)-2--4-methylpentan-1-ol

Chemical Property:

Purity/Quality:

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Technology Process of (2S)-2--4-methylpentan-1-ol

There total 7 articles about (2S)-2--4-methylpentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

N-(benzyloxycarbonyl)-phenylalanine-N-hydroxysuccinimide ester (3397-32-8) + (S)-2-amino-4-methylpentan-1-ol (7533-40-6,14438-11-0) → (2S)-2--4-methylpentan-1-ol (111633-84-2)

Guidance literature:

In 1,4-dioxane; for 12h; Ambient temperature;

Reference yield: 45.0%

(S)-2-amino-4-methylpentan-1-ol (7533-40-6,14438-11-0) + (S)-benzyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-yl)carbamate (769922-77-2) → (2S)-2--4-methylpentan-1-ol (111633-84-2)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 6h;

DOI:10.1039/b905730g

Reference yield: 7.0%

Cbz-L-Phe-L-Leu-OMe (3850-45-1) → {(S)-1-[((S)-1-Hydroxymethyl-3-methyl-butylamino)-methyl]-2-phenyl-ethyl}-carbamic acid benzyl ester + (S)-2-((S)-2-Benzyloxycarbonylamino-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester + (2S)-2--4-methylpentan-1-ol (111633-84-2)

Guidance literature:

With borane; In tetrahydrofuran; at 0 ℃; for 10h;

DOI:10.1246/bcsj.60.267

upstream raw materials:

Cbz-L-Phe-L-Leu-OMe

N-(benzyloxycarbonyl)-phenylalanine-N-hydroxysuccinimide ester

(S)-2-amino-4-methylpentan-1-ol

N-Cbz-L-Phe

Downstream raw materials:

(2S,3S)-3--5-methylhexan-2-ol

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