Technology Process of C25H24N4O5
There total 4 articles about C25H24N4O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H26N4O5;
With
potassium trimethylsilonate;
In
tetrahydrofuran;
at 20 ℃;
With
hydrogenchloride; water;
DOI:10.1021/bc200424r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; tin(II) chloride dihdyrate / methanol; water / 2 h / Reflux
2.1: sulfuric acid; sodium nitrite / acetic acid / 3.5 h / 0 - 20 °C
2.2: 1 h / 0 °C
2.3: 3 h / 0 - 10 °C
3.1: potassium trimethylsilonate / tetrahydrofuran / 20 °C
With
hydrogenchloride; tin(II) chloride dihdyrate; sulfuric acid; potassium trimethylsilonate; sodium nitrite;
In
tetrahydrofuran; methanol; water; acetic acid;
DOI:10.1021/bc200424r
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sulfuric acid; sodium nitrite / acetic acid / 3.5 h / 0 - 20 °C
1.2: 1 h / 0 °C
1.3: 3 h / 0 - 10 °C
2.1: potassium trimethylsilonate / tetrahydrofuran / 20 °C
With
sulfuric acid; potassium trimethylsilonate; sodium nitrite;
In
tetrahydrofuran; acetic acid;
DOI:10.1021/bc200424r