(salicylaldehyde benzoyl hydrazonato)copper(II) monochloride monohydrate

Base Information

• Chemical Name: (salicylaldehyde benzoyl hydrazonato)copper(II) monochloride monohydrate
• CAS No.: 176021-01-5
• Molecular Formula: C₁₄H₁₃ClCuN₂O₃
• Molecular Weight: 356.268
• Mol file: 176021-01-5.mol

Synonyms:

Chemical Property of (salicylaldehyde benzoyl hydrazonato)copper(II) monochloride monohydrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (salicylaldehyde benzoyl hydrazonato)copper(II) monochloride monohydrate

There total 2 articles about (salicylaldehyde benzoyl hydrazonato)copper(II) monochloride monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

copper(II) choride dihydrate + salicylaldehyde benzoylhydrazone (3232-37-9,71112-98-6) → (salicylaldehyde benzoyl hydrazonato)copper(II) monochloride monohydrate (56679-53-9,285981-32-0,176021-01-5,83614-45-3)

Guidance literature:

In water; salicylaldehyde benzoyl hydrazone suspended in soln. CuCl2*2H2O in water and stirred at room temp. for 4 days; solid filtered off, washed with water and acetone and dried under vac.;

DOI:10.1016/S0020-1693(00)85058-6

Reference yield:

copper(II) choride dihydrate + (E)-N'-(2-hydroxybenzylidene)benzohydrazide (71112-98-6) → chloro(salicylaldehyde benzoylhydrazonato)copper(II) monohydrate (176021-01-5,285981-32-0,56679-53-9,83614-45-3)

Guidance literature:

In methanol; Reflux;

DOI:10.1016/j.ejmech.2018.07.022

upstream raw materials:

(E)-N'-(2-hydroxybenzylidene)benzohydrazide

salicylaldehyde benzoylhydrazone