Technology Process of C26H30
There total 5 articles about C26H30 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: aluminum (III) chloride / dichloromethane / 40 °C
2: potassium hydroxide; hydrazine / diethylene glycol / 180 °C
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 60 °C
4: water; potassium hydroxide / tetrahydrofuran; methanol
With
aluminum (III) chloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; water; triethylamine; triphenylphosphine; potassium hydroxide; hydrazine;
In
tetrahydrofuran; methanol; dichloromethane; diethylene glycol;
1: Friedel-Crafts acylation / 2: Wolff-Kishner reduction / 3: Sonogashira coupling;
DOI:10.1021/ma300430e
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 60 °C
2: water; potassium hydroxide / tetrahydrofuran; methanol
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; water; triethylamine; triphenylphosphine; potassium hydroxide;
In
tetrahydrofuran; methanol;
1: Sonogashira coupling;
DOI:10.1021/ma300430e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide; hydrazine / diethylene glycol / 180 °C
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 60 °C
3: water; potassium hydroxide / tetrahydrofuran; methanol
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; water; triethylamine; triphenylphosphine; potassium hydroxide; hydrazine;
In
tetrahydrofuran; methanol; diethylene glycol;
1: Wolff-Kishner reduction / 2: Sonogashira coupling;
DOI:10.1021/ma300430e