2,2-dicyclohexyl-1,3-dioxa-2-stannolane

Base Information

• Chemical Name: 2,2-dicyclohexyl-1,3-dioxa-2-stannolane
• CAS No.: 53723-71-0
• Molecular Formula: C₁₄H₂₆O₂Sn
• Molecular Weight: 345.069

Synonyms:

Chemical Property of 2,2-dicyclohexyl-1,3-dioxa-2-stannolane

Chemical Property:

Purity/Quality:

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Technology Process of 2,2-dicyclohexyl-1,3-dioxa-2-stannolane

There total 1 articles about 2,2-dicyclohexyl-1,3-dioxa-2-stannolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

dicyclohexyltin oxide + ethylene glycol (107-21-1) → 2,2-dicyclohexyl-1,3-dioxa-2-stannolane (53723-71-0)

Guidance literature:

In cyclohexane; refluxing (2 h, azeotropic water removal), evapn., washing (EtOH); crystn. (toluene), drying (vac., 60°C);

DOI:10.1016/0022-328X(94)05356-G

Reference yield: 77.0%

2,2-dicyclohexyl-1,3-dioxa-2-stannolane (53723-71-0) + borane tetrahydrofuran → dicyclohexyltin dihydride (7529-52-4)

Guidance literature:

In cyclohexane; N2-atmosphere; dropwise addn. of excess borane complex in THF (15 min., room temp.), stirring (1-3 h), addn. of water, drying (MgSO4); evapn., distn.;

DOI:10.1016/0022-328X(94)05356-G

upstream raw materials:

ethylene glycol

Downstream raw materials:

dicyclohexyltin dihydride

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