C₃₈H₄₈BrN₅O₆

Base Information

Chemical Name:C₃₈H₄₈BrN₅O₆
CAS No.:1266683-56-0
Molecular Formula:C₃₈H₄₈BrN₅O₆
Molecular Weight:750.733
Hs Code.:

C<sub>38</sub>H<sub>48</sub>BrN<sub>5</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₃₈H₄₈BrN₅O₆

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Technology Process of C₃₈H₄₈BrN₅O₆

There total 18 articles about C₃₈H₄₈BrN₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1266683-58-2
3-bromo-5-isobutoxyaniline

: 1266683-67-3
C₂₈H₃₅ClN₄O₅

: 1266683-56-0
C₃₈H₄₈BrN₅O₆

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;
DOI:10.1002/chem.201001560

Reference yield:

: 1266683-57-1
1-azido-3-bromo-5-isobutoxybenzene

: 1266683-56-0
C₃₈H₄₈BrN₅O₆

Guidance literature:: Multi-step reaction with 8 steps

1: sodium tetrahydroborate / methanol / 20 °C

2: 1,4-dioxane / 52 °C

3: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine / 48 h / 78 °C / Inert atmosphere

4: sodium hydride / toluene / 1 h / Reflux

5: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 32 °C / Inert atmosphere; Darkness

6: water; sodium hydroxide / tetrahydrofuran / 5 h / 20 °C

7: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 20 °C

8: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With sodium tetrahydroborate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; water; sodium hydride; copper(II) sulfate; sodium L-ascorbate; diisopropylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene; tert-butyl alcohol; 3: Sonogashira coupling;
DOI:10.1002/chem.201001560

Reference yield:

: 918904-37-7
3,5-dibromo-1-isobutoxybenzene

: 1266683-56-0
C₃₈H₄₈BrN₅O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: n-butyllithium / tetrahydrofuran / -78 - -30 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / methanol / 20 °C

3.1: 1,4-dioxane / 52 °C

4.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine / 48 h / 78 °C / Inert atmosphere

5.1: sodium hydride / toluene / 1 h / Reflux

6.1: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 32 °C / Inert atmosphere; Darkness

7.1: water; sodium hydroxide / tetrahydrofuran / 5 h / 20 °C

8.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 20 °C

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With sodium tetrahydroborate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; water; sodium hydride; copper(II) sulfate; sodium L-ascorbate; diisopropylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene; tert-butyl alcohol; 4.1: Sonogashira coupling;
DOI:10.1002/chem.201001560