1,3-Dibromo-5-isobutoxybenzene

Base Information

• Chemical Name: 1,3-Dibromo-5-isobutoxybenzene
• CAS No.: 918904-37-7
• Molecular Formula: C10H12Br2O
• Molecular Weight: 308.013
• Mol file: 918904-37-7.mol

Synonyms:3,5-dibromo-1-isobutoxybenzene;Benzene,1,3-dibromo-5-(2-methylpropoxy);1,3-dibromo-5-isobutoxy-benzene;

Chemical Property of 1,3-Dibromo-5-isobutoxybenzene

Chemical Property:

• PSA: 9.23000
• LogP: 4.24640

Purity/Quality:

99% ^*data from raw suppliers

1,3-Dibromo-5-isobutoxybenzene 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Dibromo-5-isobutoxybenzene

There total 4 articles about 1,3-Dibromo-5-isobutoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.1%

Isobutyl iodide (513-38-2) + 3,5-dibromophenol (626-41-5) → 3,5-dibromo-1-isobutoxybenzene (918904-37-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 76 ℃;

DOI:10.1002/chem.201001560

Reference yield: 90.0%

→ 3,5-dibromo-1-isobutoxybenzene (918904-37-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 5h;

Reference yield:

i-pentyl bromide (107-82-4) → 3,5-dibromo-1-isobutoxybenzene (918904-37-7)

Guidance literature:

3,5-dibromophenol; With potassium hydroxide; benzyltri(n-butyl)ammonium chloride; In water; toluene; at 85 ℃;

i-pentyl bromide; In water; toluene; at 85 ℃; for 21h;

upstream raw materials:

i-pentyl bromide

Isobutyl iodide

3,5-dibromophenol

Pentabromophenol

Downstream raw materials:

N-Boc-3-bromo-5-isobutoxyaniline

N-Boc-3-(3-hydroxy-3-methylbut-1-ynyl)-5-isobutoxyaniline

N-Boc-3-ethynyl-5-isobutoxyaniline

methyl 3-(4-(3-(N-Boc-amino)-5-isobutoxyphenyl)-1H-1,2,3-triazol-1-yl)-5-isobutoxybenzoate

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