1,3-diiodo-2,4-bis(2,4,6-tri-tertbutylphenyl)-cyclo-1,3-distiba-2,4-diazane

Base Information

Chemical Name:1,3-diiodo-2,4-bis(2,4,6-tri-tertbutylphenyl)-cyclo-1,3-distiba-2,4-diazane
CAS No.:1262336-64-0
Molecular Formula:C₃₆H₅₈I₂N₂Sb₂
Molecular Weight:1016.18
Hs Code.:

Synonyms:

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Chemical Property of 1,3-diiodo-2,4-bis(2,4,6-tri-tertbutylphenyl)-cyclo-1,3-distiba-2,4-diazane

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Technology Process of 1,3-diiodo-2,4-bis(2,4,6-tri-tertbutylphenyl)-cyclo-1,3-distiba-2,4-diazane

There total 1 articles about 1,3-diiodo-2,4-bis(2,4,6-tri-tertbutylphenyl)-cyclo-1,3-distiba-2,4-diazane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 16029-98-4
trimethylsilyl iodide

: 869482-79-1
1,3-ditriflate-2,4-bis(2,4,6-tri-tertbutylphenyl)-cyclo-1,3-distiba-2,4-diazane

: 1262336-64-0
1,3-diiodo-2,4-bis(2,4,6-tri-tertbutylphenyl)-cyclo-1,3-distiba-2,4-diazane

Guidance literature:: In dichloromethane; byproducts: Me3SiOTf; Schlenk techniques used under Ar, Me3SiI added to to stirred suspn. of(TfO-Sb(μ-N-2,4,6-tri-tBu-phenyl))2 in CH2Cl2 for >5 min at ambient temp., stirred for 30 min; solvent removed, dried for 2 h in vac., washed with n-hexane, dried in vac.; XRD;
DOI:10.1002/ejic.201000885

Reference yield: 78.0%

: 1262336-64-0
1,3-diiodo-2,4-bis(2,4,6-tri-tertbutylphenyl)-cyclo-1,3-distiba-2,4-diazane

: 11113-87-4
silver fluoride

: 1262336-60-6
1,3-difluoro-2,4-bis(2,4,6-tri-tertbutylphenyl)-cyclo-1,3-distiba-2,4-diazane

Guidance literature:: In tetrahydrofuran; byproducts: silver iodide; Schlenk techniques used under Ar, AgF added to to stirred suspn. of(I-Sb(μ-N-2,4,6-tri-tBu-phenyl))2 in THF, stirred for 8 h at ambient temp.; solvent removed, dried for 30 min in vac., washed with n-hexane, extracted with THF, solvent removed, dried in vac. for 6 h; XRD;
DOI:10.1002/ejic.201000885