hexadecyl caffeate

Base Information

• Chemical Name: hexadecyl caffeate
• CAS No.: 69573-61-1
• Molecular Formula: C₂₅H₄₀O₄
• Molecular Weight: 404.59
• Mol file: 69573-61-1.mol

Synonyms:

Chemical Property of hexadecyl caffeate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of hexadecyl caffeate

There total 3 articles about hexadecyl caffeate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Hexadecanol (36653-82-4,124-29-8) + caffeic acid (331-39-5,501-16-6) → hexadecyl caffeate (69573-61-1)

Guidance literature:

With sulfuric acid; In tetrahydrofuran; at 55 ℃; Darkness; Sealed tube;

DOI:10.1021/jf500588s

Reference yield:

1-Hexadecanol (36653-82-4,124-29-8) → hexadecyl caffeate (69573-61-1)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 4 h

2: 3-amino propanoic acid; pyridine / 24 h / 60 °C

With pyridine; 3-amino propanoic acid; In toluene; 2: |Knoevenagel Condensation;

DOI:10.1039/c6ra18282h

Reference yield:

3-(hexadecyloxy)-3-oxopropanoic acid (1002-58-0) + 3,4-dihydroxybenzaldehyde (139-85-5) → hexadecyl caffeate (69573-61-1)

Guidance literature:

With pyridine; 3-amino propanoic acid; at 60 ℃; for 24h;

DOI:10.1039/c6ra18282h

upstream raw materials:

1-Hexadecanol

caffeic acid

3-(hexadecyloxy)-3-oxopropanoic acid

3,4-dihydroxybenzaldehyde