6-amino-4-Cinnolinol

Base Information

• Chemical Name: 6-amino-4-Cinnolinol
• CAS No.: 854897-28-2
• Molecular Formula: C₈H₇N₃O
• Molecular Weight: 161.163
• Mol file: 854897-28-2.mol

Synonyms:

Chemical Property of 6-amino-4-Cinnolinol

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-amino-4-Cinnolinol

There total 8 articles about 6-amino-4-Cinnolinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-nitro-1H-cinnolin-4-one (86222-55-1) → 6-amino-1H-cinnolin-4-one (854897-28-2)

Guidance literature:

With water; iron; acetic acid;

DOI:10.1039/jr9450000512 DOI:10.1021/jo01174a018

Reference yield:

1-(2-amino-5-nitro-phenyl)ethanone (32580-41-9) → 6-amino-1H-cinnolin-4-one (854897-28-2)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid; aqueous H₂SO₄ / Diazotization_.anschliessend Erwaermen

2: iron-powder; water; acetic acid

With sulfuric acid; water; iron; acetic acid;

DOI:10.1039/jr9450000512 DOI:10.1021/jo01174a018

Reference yield:

N-(2-acetyl-4-nitro-phenyl)-acetamide (41019-20-9) → 6-amino-1H-cinnolin-4-one (854897-28-2)

Guidance literature:

Multi-step reaction with 3 steps

1: aqueous hydrochloric acid

2: acetic acid; aqueous H₂SO₄ / Diazotization_.anschliessend Erwaermen

3: iron-powder; water; acetic acid

With hydrogenchloride; sulfuric acid; water; iron; acetic acid;

DOI:10.1021/jo01174a018

upstream raw materials:

6-nitro-1H-cinnolin-4-one

1-(2-amino-5-nitro-phenyl)ethanone

N-(2-acetyl-4-nitro-phenyl)-acetamide

N-(2-acetylphenyl)acetamide