2,3,8,9-Tetramethoxy-4b,10b,11,12-tetrahydrobenzo[c]phenanthridine

Base Information

Chemical Name:2,3,8,9-Tetramethoxy-4b,10b,11,12-tetrahydrobenzo[c]phenanthridine
CAS No.:54785-17-0
Molecular Formula:C₂₁H₂₃NO₄
Molecular Weight:353.418
Hs Code.:
NSC Number:166716
DSSTox Substance ID:DTXSID40304655

Synonyms:54785-17-0;NSC166716;DTXSID40304655;2,3,8,9-tetramethoxy-4b,10b,11,12-tetrahydrobenzo[c]phenanthridine;NSC-166716

Suppliers and Price of 2,3,8,9-Tetramethoxy-4b,10b,11,12-tetrahydrobenzo[c]phenanthridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 2,3,8,9-Tetramethoxy-4b,10b,11,12-tetrahydrobenzo[c]phenanthridine

Chemical Property:

Vapor Pressure:6.39E-09mmHg at 25°C
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:353.16270821
Heavy Atom Count:26
Complexity:512

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C2C3C(CCC2=C1)C4=CC(=C(C=C4C=N3)OC)OC)OC

Technology Process of 2,3,8,9-Tetramethoxy-4b,10b,11,12-tetrahydrobenzo[c]phenanthridine

There total 12 articles about 2,3,8,9-Tetramethoxy-4b,10b,11,12-tetrahydrobenzo[c]phenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 858798-43-3
N-[2-(3,4-dimethoxy-phenyl)-6,7-dimethoxy-1,2,3,4-tetrahydro-[1]naphthyl]-formamide

: 54785-17-0
2,3,8,9-tetramethoxy-4b,10b,11,12-tetrahydro-benzo[c]phenanthridine

Guidance literature:: With toluene; trichlorophosphate;

Reference yield:

: 94685-52-6
2,4-bis(3,4-dimethoxyphenyl)-4-butyronitrilone

: 54785-17-0
2,3,8,9-tetramethoxy-4b,10b,11,12-tetrahydro-benzo[c]phenanthridine

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid; sulfuric acid

2: aq.-ethanolic NaOH-solution

3: amalgamated zinc; aqueous hydrochloric acid; toluene / weiteres Reagenz: Essigsaeure

4: POCl₃

6: phosphoryl chloride; toluene

With hydrogenchloride; sodium hydroxide; amalgamated zinc; sulfuric acid; acetic acid; toluene; trichlorophosphate;

Reference yield:

: 94577-55-6
2,4-bis-(3,4-dimethoxy-phenyl)-4-oxo-butyric acid amide

: 54785-17-0
2,3,8,9-tetramethoxy-4b,10b,11,12-tetrahydro-benzo[c]phenanthridine

Guidance literature:: Multi-step reaction with 5 steps

1: aq.-ethanolic NaOH-solution

2: amalgamated zinc; aqueous hydrochloric acid; toluene / weiteres Reagenz: Essigsaeure

3: POCl₃

5: phosphoryl chloride; toluene

With hydrogenchloride; sodium hydroxide; amalgamated zinc; toluene; trichlorophosphate;