CF₃O₃S^(1-)*C₂₈H₄₀NO⁽¹⁺⁾

Base Information

• Chemical Name: CF₃O₃S^(1-)*C₂₈H₄₀NO⁽¹⁺⁾
• CAS No.: 1380325-71-2
• Molecular Formula: CF₃O₃S*C₂₈H₄₀NO
• Molecular Weight: 555.702

Synonyms:

Chemical Property of CF₃O₃S^(1-)*C₂₈H₄₀NO⁽¹⁺⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of CF₃O₃S^(1-)*C₂₈H₄₀NO⁽¹⁺⁾

There total 7 articles about CF₃O₃S^(1-)*C₂₈H₄₀NO⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-N-[(1S,2S)-2-hydroxy-1,2-diphenylethyl]-N,2-dimethyl-2-neopentylheptanamide (1380325-69-8) → CF3O3S(1-)*C28H40NO(1+) (1380325-71-2)

Guidance literature:

With pyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at 0 ℃; for 0.166667h; optical yield given as %de; Inert atmosphere;

DOI:10.1002/anie.201200370

Reference yield:

N-[(1S,2S)-2-hydroxy-1,2-diphenylethyl]-N-methyl-2-methyleneheptanamide (1380325-30-3) → CF3O3S(1-)*C28H40NO(1+) (1380325-71-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: methyllithium; lithium chloride / tetrahydrofuran; formaldehyde diethyl acetal / 0.17 h / -78 °C / Inert atmosphere

1.2: 0.33 h / -78 - -40 °C / Inert atmosphere

1.3: 6 h / -40 °C / Inert atmosphere

2.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

With pyridine; trifluoromethylsulfonic anhydride; methyllithium; lithium chloride; In tetrahydrofuran; formaldehyde diethyl acetal; dichloromethane;

DOI:10.1002/anie.201200370

Reference yield:

N-[(1S,2S)-2-hydroxy-1,2-diphenylethyl]formamide (301191-47-9) → CF3O3S(1-)*C28H40NO(1+) (1380325-71-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 22.17 h / 0 - 23 °C / Inert atmosphere

2.1: benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 23 °C / Inert atmosphere

3.1: methyllithium; lithium chloride / tetrahydrofuran; formaldehyde diethyl acetal / 0.17 h / -78 °C / Inert atmosphere

3.2: 0.33 h / -78 - -40 °C / Inert atmosphere

3.3: 6 h / -40 °C / Inert atmosphere

4.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; trifluoromethylsulfonic anhydride; methyllithium; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; diethyl ether; formaldehyde diethyl acetal; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/anie.201200370

upstream raw materials:

N-[(1S,2S)-2-hydroxy-1,2-diphenylethyl]-N-methyl-2-methyleneheptanamide

(R)-N-[(1S,2S)-2-hydroxy-1,2-diphenylethyl]-N,2-dimethyl-2-neopentylheptanamide

N-[(1S,2S)-2-hydroxy-1,2-diphenylethyl]formamide

(1S,2S)-2-amino-1,2-diphenylethanol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1380325-71-2 CF₃O₃S^(1-)*C₂₈H₄₀NO⁽¹⁺⁾

Send

Send

Metric Ton KG G Pound L ML

Send

Send