C₂₁H₁₉F₄N₃O₄S

Base Information

Chemical Name:C₂₁H₁₉F₄N₃O₄S
CAS No.:1622844-68-1
Molecular Formula:C₂₁H₁₉F₄N₃O₄S
Molecular Weight:485.459
Hs Code.:

C<sub>21</sub>H<sub>19</sub>F<sub>4</sub>N<sub>3</sub>O<sub>4</sub>S

Synonyms:

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Chemical Property of C₂₁H₁₉F₄N₃O₄S

Chemical Property:

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Technology Process of C₂₁H₁₉F₄N₃O₄S

There total 5 articles about C₂₁H₁₉F₄N₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13331-23-2
fur-2-ylboronic acid

: 935513-62-5
C₁₇H₁₆ClF₄N₃O₃S

: 1622844-68-1
C₂₁H₁₉F₄N₃O₄S

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; toluene; at 100 ℃; for 1h; Microwave irradiation;
DOI:10.1016/j.bmcl.2014.05.072

Reference yield:

: 386704-06-9
2-chloro-6-(trifluoromethyl)nicotinonitrile

: 1622844-68-1
C₂₁H₁₉F₄N₃O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylsulfide borane complex / tetrahydrofuran / Reflux

2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; N,N-dimethyl-formamide

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene; ethanol / 1 h / 100 °C / Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimethylsulfide borane complex; sodium carbonate; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene; 3: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.05.072

Reference yield:

: 771572-85-1
(2-chloro-6-(trifluoromethyl)pyridin-3-yl)methanamine

: 1622844-68-1
C₂₁H₁₉F₄N₃O₄S

Guidance literature:: Multi-step reaction with 2 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; N,N-dimethyl-formamide

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene; ethanol / 1 h / 100 °C / Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene; 2: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.05.072