(R)-2-butyl-2-methylcyclohexanone

Base Information

Chemical Name:(R)-2-butyl-2-methylcyclohexanone
CAS No.:83606-10-4
Molecular Formula:C₁₁H₂₀O
Molecular Weight:168.279
Hs Code.:

Synonyms:

Suppliers and Price of (R)-2-butyl-2-methylcyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (R)-2-butyl-2-methylcyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (R)-2-butyl-2-methylcyclohexanone

There total 8 articles about (R)-2-butyl-2-methylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 147650-39-3
(1R,6R)-1-(Chloroacetoxy)-6-butylbicyclo<4.1.0>heptane

: 83606-10-4
(R)-2-butyl-2-methylcyclohexanone

: (S)-2-Butyl-2-methylcyclohexanone

Guidance literature:: With sodium hydroxide; In methanol; at 60 ℃; for 4h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00058a046

Reference yield:

: 147583-53-7
(1S,6S)-1-Hydroxyx-6-butylbicyclo<4.1.0>heptane

: 83606-10-4
(R)-2-butyl-2-methylcyclohexanone

: (S)-2-Butyl-2-methylcyclohexanone

Guidance literature:: With sodium hydroxide; In methanol; at 60 ℃; for 4h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00058a046

Reference yield:

: 1728-38-7
methyl enol ether of 2-methylcyclohexanone

: 83606-10-4
(R)-2-butyl-2-methylcyclohexanone

Guidance literature:: Multi-step reaction with 7 steps

2: 95 percent / 2) 40percent potassium hydroxide / 1) a) petroleum/ether, 20 deg C, 15 min, b) 4 h, 2) a) 4 h, b) methanol/water, 16 h

3: bromine / CCl₄ / 0 °C

4: 84 percent / potassium t-butoxide / 2-methyl-propan-2-ol / 10 h / 10 °C

5: 67 percent / sodamide / 1) petroleum ether, 2) without solvent, 130 deg C

6: 94 percent / 1) oxalyl chloride, dimethyl sulphoxide, 2) triethylamine / CH₂Cl₂ / 1) -67 deg C, 20 min, 2) warming to room temperature

7: H₂ / 5percent palladium charcoal / ethanol / 0.17 h

With potassium hydroxide; oxalyl dichloride; potassium tert-butylate; hydrogen; bromine; sodium amide; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In tetrachloromethane; ethanol; dichloromethane; tert-butyl alcohol;