Technology Process of C28H50O6
There total 6 articles about C28H50O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / toluene / Reflux
2: Schwartz's reagent; methylmagnesium chloride; copper(l) iodide / tetrahydrofuran / -20 °C
3: pyridinium p-toluenesulfonate / dichloromethane
4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran
With
copper(l) iodide; Schwartz's reagent; tetrabutyl ammonium fluoride; methylmagnesium chloride; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; acetic acid;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2012.10.083
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Schwartz's reagent; methylmagnesium chloride; copper(l) iodide / tetrahydrofuran / -20 °C
2: pyridinium p-toluenesulfonate / dichloromethane
3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran
With
copper(l) iodide; Schwartz's reagent; tetrabutyl ammonium fluoride; methylmagnesium chloride; pyridinium p-toluenesulfonate; acetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.10.083
- Guidance literature:
-
Multi-step reaction with 4 steps
1: diethyl (2R,3R)-tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane
2: Schwartz's reagent; methylmagnesium chloride; copper(l) iodide / tetrahydrofuran / -20 °C
3: pyridinium p-toluenesulfonate / dichloromethane
4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; copper(l) iodide; Schwartz's reagent; diethyl (2R,3R)-tartrate; tetrabutyl ammonium fluoride; methylmagnesium chloride; pyridinium p-toluenesulfonate; acetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.10.083