6-<3-(4-sulfophenyl)-2-triazen-1-yl>purine ribonucleoside 5'-phosphate

Base Information

• Chemical Name: 6-<3-(4-sulfophenyl)-2-triazen-1-yl>purine ribonucleoside 5'-phosphate
• CAS No.: 79982-46-0
• Molecular Formula: C₁₆H₁₈N₇O₁₀PS
• Molecular Weight: 531.4
• Mol file: 79982-46-0.mol

Synonyms:

Chemical Property of 6-<3-(4-sulfophenyl)-2-triazen-1-yl>purine ribonucleoside 5'-phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 6-<3-(4-sulfophenyl)-2-triazen-1-yl>purine ribonucleoside 5'-phosphate

There total 3 articles about 6-<3-(4-sulfophenyl)-2-triazen-1-yl>purine ribonucleoside 5'-phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-sulfobenzenediazonium chloride (6118-33-8) + 5'-adenosine monophosphate (61-19-8,24937-83-5,67583-85-1) → 6-<3-(4-sulfophenyl)-2-triazen-1-yl>purine ribonucleoside 5'-phosphate (79982-46-0,77079-62-0)

Guidance literature:

In sodium hydroxide; for 0.25h; Title compound not separated from byproducts; Ambient temperature; pH 8.0 and 10.5;

DOI:10.1021/jo00342a014

Reference yield:

C16H17BrN7O7P (77079-61-9) → C16H18N7O10PS (77079-62-0,79982-46-0)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH / 72 h / 90 °C / pH 9-10

2: 1.) conc. HCl, NaNO₂, 2.) NaOH / 1.) H₂O, 0 deg C, 2.) pH 10-11, 10 min

With hydrogenchloride; sodium hydroxide; sodium nitrite;

DOI:10.1021/jo00324a001

Reference yield:

5'-adenosine monophosphate (61-19-8,24937-83-5,67583-85-1) + 4-aminobenzene sulfonic acid (121-57-3,856062-06-1) → C16H18N7O10PS (77079-62-0,79982-46-0)

Guidance literature:

With hydrogenchloride; sodium hydroxide; sodium nitrite; Yield given. Multistep reaction; 1.) H₂O, 0 deg C, 2.) pH 10-11, 10 min;

DOI:10.1021/jo00324a001

upstream raw materials:

p-sulfobenzenediazonium chloride

5'-adenosine monophosphate

4-aminobenzene sulfonic acid

C₁₆H₁₇BrN₇O₇P