9-(2-deoxy-5-O-phosphonopentofuranosyl)-2-{[(1S,2S,3R,4S)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydrotetraphen-1-yl]amino}-3,9-dihydro-6H-purin-6-one

Base Information

Chemical Name:9-(2-deoxy-5-O-phosphonopentofuranosyl)-2-{[(1S,2S,3R,4S)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydrotetraphen-1-yl]amino}-3,9-dihydro-6H-purin-6-one
CAS No.:133645-03-1
Molecular Formula:C₂₉H₂₉N₅O₇
Molecular Weight:559.579
Hs Code.:

9-(2-deoxy-5-O-phosphonopentofuranosyl)-2-{[(1S,2S,3R,4S)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydrotetraphen-1-yl]amino}-3,9-dihydro-6H-purin-6-one

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(2-deoxy-5-O-phosphonopentofuranosyl)-2-{[(1S,2S,3R,4S)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydrotetraphen-1-yl]amino}-3,9-dihydro-6H-purin-6-one

Chemical Property:

Vapor Pressure:0mmHg at 25°C

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Technology Process of 9-(2-deoxy-5-O-phosphonopentofuranosyl)-2-{[(1S,2S,3R,4S)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydrotetraphen-1-yl]amino}-3,9-dihydro-6H-purin-6-one

There total 3 articles about 9-(2-deoxy-5-O-phosphonopentofuranosyl)-2-{[(1S,2S,3R,4S)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydrotetraphen-1-yl]amino}-3,9-dihydro-6H-purin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133645-02-0,63057-64-7,64625-66-7
(+/-)-trans-3,4-Dihydroxy-anti-1,2-epoxy-7-methyl-1,2,3,4-tetrahydrobenz anthracene

: 902-04-5
2'-deoxyguanosine 5'-monophosphate

: 133551-46-9,133645-03-1,133645-07-5,133646-13-6
Phosphoric acid mono-{(2R,3S,5R)-3-hydroxy-5-[6-oxo-2-(2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydro-benzo[a]anthracen-1-ylamino)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-2-ylmethyl} ester

Guidance literature:: With tris-HCl-buffer; In acetone; at 37 ℃;
DOI:10.1021/jo00013a020

Reference yield:

: 133551-46-9,133645-03-1,133645-07-5,133646-13-6
Phosphoric acid mono-{(2R,3S,5R)-3-hydroxy-5-[6-oxo-2-(2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydro-benzo[a]anthracen-1-ylamino)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-2-ylmethyl} ester

: 133645-03-1
9-((2R,4S,5R)-4-Hydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-2-((1S,2S,3R,4S)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydro-benzo[a]anthracen-1-ylamino)-1,9-dihydro-purin-6-one

: 133646-13-6
9-((2R,4S,5R)-4-Hydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-2-((1S,2R,3S,4R)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydro-benzo[a]anthracen-1-ylamino)-1,9-dihydro-purin-6-one

: 133551-46-9
9-((2R,4S,5R)-4-Hydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-2-((1R,2S,3R,4S)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydro-benzo[a]anthracen-1-ylamino)-1,9-dihydro-purin-6-one

: 133645-07-5
9-((2R,4S,5R)-4-Hydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-2-((1R,2R,3S,4R)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydro-benzo[a]anthracen-1-ylamino)-1,9-dihydro-purin-6-one

Guidance literature:: alkaline phosphatase;
DOI:10.1021/jo00013a020

Reference yield:

: 902-04-5
2'-deoxyguanosine 5'-monophosphate

: 133645-03-1
9-((2R,4S,5R)-4-Hydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-2-((1S,2S,3R,4S)-2,3,4-trihydroxy-7-methyl-1,2,3,4-tetrahydro-benzo[a]anthracen-1-ylamino)-1,9-dihydro-purin-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: Tris-HCl-buffer / acetone / 37 °C

2: alkaline phosphatase

With tris-HCl-buffer; In acetone;
DOI:10.1021/jo00013a020