Technology Process of C32H29F3N6OS
There total 7 articles about C32H29F3N6OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium hydroxide; water / tetrahydrofuran
2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine
3: trifluoroacetic acid
With
water; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran;
DOI:10.1016/j.bmcl.2013.04.009
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium carbonate / 90 °C
2: 1,4-dioxane / 90 °C
3: iron; ammonium chloride / ethanol; water / Reflux
4: acetic acid / 0.33 h / 120 °C
5: lithium hydroxide; water / tetrahydrofuran
6: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine
7: trifluoroacetic acid
With
water; iron; potassium carbonate; ammonium chloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water;
DOI:10.1016/j.bmcl.2013.04.009
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium carbonate / 90 °C
2: 1,4-dioxane / 90 °C
3: iron; ammonium chloride / ethanol; water / Reflux
4: acetic acid / 0.33 h / 120 °C
5: lithium hydroxide; water / tetrahydrofuran
6: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine
7: trifluoroacetic acid
With
water; iron; potassium carbonate; ammonium chloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water;
DOI:10.1016/j.bmcl.2013.04.009