(2R)-4-(1-ethoxyethoxy)-2-((methoxymethoxy)methyl)-2-methylbutanal

Base Information

Chemical Name:(2R)-4-(1-ethoxyethoxy)-2-((methoxymethoxy)methyl)-2-methylbutanal
CAS No.:890027-54-0
Molecular Formula:C₁₂H₂₄O₅
Molecular Weight:248.32
Hs Code.:

Synonyms:

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Chemical Property of (2R)-4-(1-ethoxyethoxy)-2-((methoxymethoxy)methyl)-2-methylbutanal

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Technology Process of (2R)-4-(1-ethoxyethoxy)-2-((methoxymethoxy)methyl)-2-methylbutanal

There total 11 articles about (2R)-4-(1-ethoxyethoxy)-2-((methoxymethoxy)methyl)-2-methylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 890027-78-8
(2S)-4-(1-ethoxyethoxy)-2-((methoxymethoxy)methyl)-2-methylbutan-1-ol

: 890027-54-0
(2R)-4-(1-ethoxyethoxy)-2-((methoxymethoxy)methyl)-2-methylbutanal

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1002/chem.201204119

Reference yield:

: 890027-41-5
(R)-2-methyl-2-(3-phenyl-2-propenyl)malonic acid monomethyl ester

: 890027-54-0
(2R)-4-(1-ethoxyethoxy)-2-((methoxymethoxy)methyl)-2-methylbutanal

Guidance literature:: Multi-step reaction with 9 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate; methanol / tetrahydrofuran / -30 - 20 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; sodium iodide / dichloromethane / Reflux; Inert atmosphere

4.1: lithium aluminium tetrahydride / diethyl ether / 0 - 20 °C / Inert atmosphere

5.1: dmap; pyridine / dichloromethane / 20 °C

6.1: ozone / methanol / -78 °C / Inert atmosphere

6.2: -78 - 0 °C / Inert atmosphere

7.1: pyridinium p-toluenesulfonate / dichloromethane / 20 °C / Inert atmosphere

8.1: methanol; potassium carbonate / 20 °C / Inert atmosphere

9.1: triethylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 0 °C / Inert atmosphere

With pyridine; methanol; dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; oxalyl dichloride; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; potassium carbonate; ozone; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 9.1: |Parikh-Doering Oxidation;
DOI:10.1002/chem.201204119

Reference yield:

: 1444378-51-1
2-methyl-2-(3-phenyl-2-propenyl)malonic acid monomethyl ester

: 890027-54-0
(2R)-4-(1-ethoxyethoxy)-2-((methoxymethoxy)methyl)-2-methylbutanal

Guidance literature:: Multi-step reaction with 10 steps

1.1: pig liver esterase / 168 h / 30 °C / pH 8 / Enzymatic reaction

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate; methanol / tetrahydrofuran / -30 - 20 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; sodium iodide / dichloromethane / Reflux; Inert atmosphere

5.1: lithium aluminium tetrahydride / diethyl ether / 0 - 20 °C / Inert atmosphere

6.1: dmap; pyridine / dichloromethane / 20 °C

7.1: ozone / methanol / -78 °C / Inert atmosphere

7.2: -78 - 0 °C / Inert atmosphere

8.1: pyridinium p-toluenesulfonate / dichloromethane / 20 °C / Inert atmosphere

9.1: methanol; potassium carbonate / 20 °C / Inert atmosphere

10.1: triethylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 0 °C / Inert atmosphere

With pyridine; methanol; dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; pig liver esterase; oxalyl dichloride; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; potassium carbonate; ozone; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 10.1: |Parikh-Doering Oxidation;
DOI:10.1002/chem.201204119