C₄₄H₆₅N₃O₂₀Si

Base Information

Chemical Name:C₄₄H₆₅N₃O₂₀Si
CAS No.:1333414-26-8
Molecular Formula:C₄₄H₆₅N₃O₂₀Si
Molecular Weight:984.094
Hs Code.:

C<sub>44</sub>H<sub>65</sub>N<sub>3</sub>O<sub>20</sub>Si

Synonyms:

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Chemical Property of C₄₄H₆₅N₃O₂₀Si

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Technology Process of C₄₄H₆₅N₃O₂₀Si

There total 14 articles about C₄₄H₆₅N₃O₂₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₃₅O₁₁N

: 1333414-26-8
C₄₄H₆₅N₃O₂₀Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: methanol; sodium methylate / 12 h / 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C

3.1: sodium hydride / 1,4-dioxane / 60 °C / Inert atmosphere

4.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.1: methanol; toluene-4-sulfonic acid / 1 h / 70 °C

5.2: 20 °C

6.1: dichloromethane / 0.42 h / -78 °C / Inert atmosphere

7.1: pyridine / dichloromethane / 0.83 h / -78 °C / Inert atmosphere

8.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 14 h / -78 - 20 °C / Inert atmosphere; Molecular sieve

9.1: hydrazinium monoacetate / methanol / 12 h / Inert atmosphere; Reflux

10.1: pyridine / 0 - 20 °C / Inert atmosphere

With pyridine; methanol; dmap; trimethylsilyl trifluoromethanesulfonate; sodium methylate; hydrazinium monoacetate; sodium hydride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; methanol; dichloromethane; acetonitrile;
DOI:10.1021/ol2021687

Reference yield:

: C₁₈H₂₇NO₇

: 1333414-26-8
C₄₄H₆₅N₃O₂₀Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C

2.1: sodium hydride / 1,4-dioxane / 60 °C / Inert atmosphere

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.1: methanol; toluene-4-sulfonic acid / 1 h / 70 °C

4.2: 20 °C

5.1: dichloromethane / 0.42 h / -78 °C / Inert atmosphere

6.1: pyridine / dichloromethane / 0.83 h / -78 °C / Inert atmosphere

7.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 14 h / -78 - 20 °C / Inert atmosphere; Molecular sieve

8.1: hydrazinium monoacetate / methanol / 12 h / Inert atmosphere; Reflux

9.1: pyridine / 0 - 20 °C / Inert atmosphere

With pyridine; methanol; dmap; trimethylsilyl trifluoromethanesulfonate; hydrazinium monoacetate; sodium hydride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; methanol; dichloromethane; acetonitrile;
DOI:10.1021/ol2021687

Reference yield:

: 77277-00-0
C₂₅H₃₁NO₇

: 1333414-26-8
C₄₄H₆₅N₃O₂₀Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / 1,4-dioxane / 60 °C / Inert atmosphere

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.1: methanol; toluene-4-sulfonic acid / 1 h / 70 °C

3.2: 20 °C

4.1: dichloromethane / 0.42 h / -78 °C / Inert atmosphere

5.1: pyridine / dichloromethane / 0.83 h / -78 °C / Inert atmosphere

6.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 14 h / -78 - 20 °C / Inert atmosphere; Molecular sieve

7.1: hydrazinium monoacetate / methanol / 12 h / Inert atmosphere; Reflux

8.1: pyridine / 0 - 20 °C / Inert atmosphere

With pyridine; methanol; dmap; trimethylsilyl trifluoromethanesulfonate; hydrazinium monoacetate; sodium hydride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/ol2021687