C₅₁H₅₀N₆O₁₁

Base Information

Chemical Name:C₅₁H₅₀N₆O₁₁
CAS No.:1446513-18-3
Molecular Formula:C₅₁H₅₀N₆O₁₁
Molecular Weight:922.992
Hs Code.:

C<sub>51</sub>H<sub>50</sub>N<sub>6</sub>O<sub>11</sub>

Synonyms:

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Chemical Property of C₅₁H₅₀N₆O₁₁

Chemical Property:

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Technology Process of C₅₁H₅₀N₆O₁₁

There total 8 articles about C₅₁H₅₀N₆O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₂₇N₅O₆

: 71989-14-5
Fmoc-(tBu)Asp-OH

: 1446513-18-3
C₅₁H₅₀N₆O₁₁

Guidance literature:: C₂₈H₂₇N₅O₆; Fmoc-(tBu)Asp-OH; With N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 18h;
DOI:10.1039/c3ob41047a

Reference yield:

: 1446512-94-2
(S)-N-((4-(2-((tert-butoxycarbonyl)amino)-2-carboxyethyl)phenoxy)carbonyl)-3-phenylsydnonimine

: 1446513-18-3
C₅₁H₅₀N₆O₁₁

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 0 °C

1.2: 18 h / 0 - 20 °C

2.1: hydrogenchloride / dichloromethane; 1,4-dioxane; water

3.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 0 °C

3.2: 18 h / 0 - 20 °C

With hydrogenchloride; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c3ob41047a

Reference yield:

: 62-53-3
aniline

: 1446513-18-3
C₅₁H₅₀N₆O₁₁

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate; sodium iodide / acetone / 12 h / 20 °C / Darkness

2.1: isopentyl nitrite / diethyl ether / 16 h / 20 °C / Darkness

2.2: 0.25 h / 20 °C

3.1: triethylamine / dichloromethane / 16 h / -20 - 20 °C

4.1: acetonitrile / 18 h / Reflux

5.1: sodium hydroxide; water / tetrahydrofuran / 20 °C

6.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 0 °C

6.2: 18 h / 0 - 20 °C

7.1: hydrogenchloride / dichloromethane; 1,4-dioxane; water

8.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 0 °C

8.2: 18 h / 0 - 20 °C

With hydrogenchloride; water; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium iodide; sodium hydroxide; isopentyl nitrite; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1039/c3ob41047a