Technology Process of C47H48N5O11P
There total 11 articles about C47H48N5O11P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 87 percent / triethylamine / methanol / 0.5 h / Ambient temperature
2: 97 percent / ammonia / methanol / Ambient temperature
3: 84 percent / toluene-4-sulphonic acid monohydrate / tetrahydrofuran / 1 h / 50 °C
4: 88 percent / 3-chloroperbenzoic acid / CH2Cl2 / 2.5 h / -5 °C
5: 70 percent / N,N-di-isopropylethylamine / N,N-dimethyl-acetamide / 28 h / 70 - 75 °C
6: 1.03 g / pyridine / 2 h / -40 °C
With
pyridine; ammonia; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl acetamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 84 percent / toluene-4-sulphonic acid monohydrate / tetrahydrofuran / 1 h / 50 °C
2: 88 percent / 3-chloroperbenzoic acid / CH2Cl2 / 2.5 h / -5 °C
3: 70 percent / N,N-di-isopropylethylamine / N,N-dimethyl-acetamide / 28 h / 70 - 75 °C
4: 1.03 g / pyridine / 2 h / -40 °C
With
pyridine; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 84 percent / toluene-4-sulphonic acid monohydrate / tetrahydrofuran / 1 h / 50 °C
2: 88 percent / 3-chloroperbenzoic acid / CH2Cl2 / 2.5 h / -5 °C
3: 70 percent / N,N-di-isopropylethylamine / N,N-dimethyl-acetamide / 28 h / 70 - 75 °C
4: 1.03 g / pyridine / 2 h / -40 °C
With
pyridine; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide;