N⁶-<<2-(4-Nitrophenyl)ethoxy>carbonyl>-9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-3'-iodo-5'-O-(monomethoxytrityl)-β-D-xylofuranosyl>adenine

Base Information

• Chemical Name: N⁶-<<2-(4-Nitrophenyl)ethoxy>carbonyl>-9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-3'-iodo-5'-O-(monomethoxytrityl)-β-D-xylofuranosyl>adenine
• CAS No.: 132849-68-4
• Molecular Formula: C₄₅H₄₉IN₆O₈Si
• Molecular Weight: 956.909

Synonyms:

Chemical Property of N⁶-<<2-(4-Nitrophenyl)ethoxy>carbonyl>-9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-3'-iodo-5'-O-(monomethoxytrityl)-β-D-xylofuranosyl>adenine

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Technology Process of N⁶-<<2-(4-Nitrophenyl)ethoxy>carbonyl>-9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-3'-iodo-5'-O-(monomethoxytrityl)-β-D-xylofuranosyl>adenine

There total 1 articles about N⁶-<<2-(4-Nitrophenyl)ethoxy>carbonyl>-9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-3'-iodo-5'-O-(monomethoxytrityl)-β-D-xylofuranosyl>adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N6-<<2-(4-Nitrophenyl)ethoxy>carbonyl>-9-<3'-deoxy-3'-iodo-5'-O-(monomethoxytrityl)-β-D-xylofuranosyl>adenine (132849-67-3) + tert-butyldimethylsilyl chloride (18162-48-6) → N6-<<2-(4-Nitrophenyl)ethoxy>carbonyl>-9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-3'-iodo-5'-O-(monomethoxytrityl)-β-D-xylofuranosyl>adenine (132849-68-4)

Guidance literature:

With pyridine; 1H-imidazole; for 31h; Ambient temperature;

DOI:10.1002/hlca.19910740104

Reference yield: 84.0%

N6-<<2-(4-Nitrophenyl)ethoxy>carbonyl>-9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-3'-iodo-5'-O-(monomethoxytrityl)-β-D-xylofuranosyl>adenine (132849-68-4) → 9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-5'-O-(monomethoxytrityl)-β-D-glycero-pent-3'-enofuranosyl>adenine (132849-79-7)

Guidance literature:

With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; for 21h; Ambient temperature;

DOI:10.1002/hlca.19910740104

upstream raw materials:

N⁶-<<2-(4-Nitrophenyl)ethoxy>carbonyl>-9-<3'-deoxy-3'-iodo-5'-O-(monomethoxytrityl)-β-D-xylofuranosyl>adenine

tert-butyldimethylsilyl chloride

Downstream raw materials:

9-<2'-O-<(tert-butyl)dimethylsilyl>-3'-deoxy-5'-O-(monomethoxytrityl)-β-D-glycero-pent-3'-enofuranosyl>adenine

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