Technology Process of di-<
-carbonylmethylen> disulfide
There total 4 articles about di-<-carbonylmethylen> disulfide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium ethyl xanthogenate;
In
dimethyl sulfoxide;
1.) 1 h, r.t. 2.) 4-5 h, 50-60 deg C;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 54 percent / Br2 / acetic acid / 1.5 h / 60 °C
2: 30 percent / potassium ethylxanthate / dimethylsulfoxide / 1.) 1 h, r.t. 2.) 4-5 h, 50-60 deg C
With
bromine; potassium ethyl xanthogenate;
In
acetic acid; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) NaNO2, 6M HCl 2) NaN3 / 1) 0 deg C, H2O 2) H2O, r.t.
2: 61 percent / 24 h / 80 °C
3: 54 percent / Br2 / acetic acid / 1.5 h / 60 °C
4: 30 percent / potassium ethylxanthate / dimethylsulfoxide / 1.) 1 h, r.t. 2.) 4-5 h, 50-60 deg C
With
hydrogenchloride; sodium azide; bromine; potassium ethyl xanthogenate; sodium nitrite;
In
acetic acid; dimethyl sulfoxide;
![2-Bromo-1-(4-[1,2,3]triazol-1-yl-phenyl)-ethanone](/Databaselist/images/loading.webp)
