N^ω-nitro-N^α-(4-nitro-benzyloxycarbonyl)-L-arginine

Base Information

Chemical Name:N^ω-nitro-N^α-(4-nitro-benzyloxycarbonyl)-L-arginine
CAS No.:183659-61-2
Molecular Formula:C₁₄H₁₈N₆O₈
Molecular Weight:398.332
Hs Code.:

<i>N</i><sup>ω</sup>-nitro-<i>N</i><sup>α</sup>-(4-nitro-benzyloxycarbonyl)-L-arginine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^ω-nitro-N^α-(4-nitro-benzyloxycarbonyl)-L-arginine

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Technology Process of N^ω-nitro-N^α-(4-nitro-benzyloxycarbonyl)-L-arginine

There total 1 articles about N^ω-nitro-N^α-(4-nitro-benzyloxycarbonyl)-L-arginine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2149-70-4,13855-78-2,38733-00-5
N-nitro-L-arginine

: 4457-32-3
4-nitrobenzyl chloroformate

: 183659-61-2
N^ω-nitro-N^α-(4-nitro-benzyloxycarbonyl)-L-arginine

Guidance literature:: With tetrahydrofuran; sodium hydroxide;
DOI:10.1021/jo01113a610

Reference yield:

: 183659-61-2
N^ω-nitro-N^α-(4-nitro-benzyloxycarbonyl)-L-arginine

: 2418-67-9
L-Arg-Gly

Guidance literature:: Multi-step reaction with 3 steps

1: chlorocarbonic acid ethyl ester; tributylamine; THF / anschliessend Behandeln mit Glycin-aethylester

2: methanol; aqueous NaOH

3: palladium/charcoal; ethanol; acetic acid

With tetrahydrofuran; methanol; sodium hydroxide; palladium on activated charcoal; tributyl-amine; ethanol; chloroformic acid ethyl ester; acetic acid;
DOI:10.1021/jo01113a610