Phosphoric acid (2R,3S,5R)-5-(4-amino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(2-amino-6-oxo-1,6-dihydro-purin-9-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester

Base Information

• Chemical Name: Phosphoric acid (2R,3S,5R)-5-(4-amino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(2-amino-6-oxo-1,6-dihydro-purin-9-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester
• CAS No.: 81539-53-9
• Molecular Formula: C₂₀H₂₇N₈O₁₀P
• Molecular Weight: 570.456

Synonyms:

Chemical Property of Phosphoric acid (2R,3S,5R)-5-(4-amino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(2-amino-6-oxo-1,6-dihydro-purin-9-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester

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Technology Process of Phosphoric acid (2R,3S,5R)-5-(4-amino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(2-amino-6-oxo-1,6-dihydro-purin-9-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester

There total 1 articles about Phosphoric acid (2R,3S,5R)-5-(4-amino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(2-amino-6-oxo-1,6-dihydro-purin-9-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C50H49N10O13P → Phosphoric acid (2R,3S,5R)-5-(4-amino-5-methyl-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S,5R)-5-(2-amino-6-oxo-1,6-dihydro-purin-9-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester (81539-53-9) + Thymidynyl-(3'->5')-2'-deoxyguanosine (4251-20-1)

Guidance literature:

With 2-pyridinealdoxime; ammonium hydroxide; acetic acid; N,N,N',N'-tetramethylguanidine; Yield given. Multistep reaction. Yields of byproduct given; 1.) 15 h at room temperature, then 3 h at 40 deg C, 2.) 15 min at room temperature. Variation of reagents, solvents, temperatures and times;

DOI:10.1016/S0040-4039(00)61903-2

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