C₆₃H₇₈N₄O₁₂SSi

Base Information

Chemical Name:C₆₃H₇₈N₄O₁₂SSi
CAS No.:131703-72-5
Molecular Formula:C₆₃H₇₈N₄O₁₂SSi
Molecular Weight:1143.48
Hs Code.:

C<sub>63</sub>H<sub>78</sub>N<sub>4</sub>O<sub>12</sub>SSi

Synonyms:

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Chemical Property of C₆₃H₇₈N₄O₁₂SSi

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Technology Process of C₆₃H₇₈N₄O₁₂SSi

There total 32 articles about C₆₃H₇₈N₄O₁₂SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4435-54-5
2-Methylene-1-butanol

: 131703-72-5,131829-83-9
C₆₃H₇₈N₄O₁₂SSi

Guidance literature:: Multi-step reaction with 10 steps

1: L-(+)-diethyl tartrate, titanium(IV) isopropoxide, tert-butyl hydroperoxide, activated 4.0-Angstroem molecular sieves / CH₂Cl₂; 2,2,4-trimethyl-pentane / 1.) -20 deg C, 4 h, 2.) -15 deg C, 12 h

2: 91 percent / copper iodide / tetrahydrofuran / 1.) -25 to -30 deg C, 6 h, 2.) -15 deg C, 12 h

3: 99 percent / p-toluenesulfonic acid / acetone / 12 h

4: 1.) ozone, 2.) triphenylphosphine / 1.) CH₂Cl₂, -78 deg C, 15 min, 2.) room temperature, 24 h

6: 110 mg / 10percent aq. HCl / methanol / 0.25 h / Heating

7: 76 percent / triethylamine / CH₂Cl₂ / 26 h

8: 92 percent / N,N-diisopropylethylamine / tetrahydrofuran / 0.25 h / 0 °C

9: tert-butyl hypochlorite, triethylamine / CH₂Cl₂ / 0.08 h / 0 °C

10: HBF₄*Et₂O, AgBF₄ / acetone / 0.08 h

With titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; tetrafluoroboric acid diethyl ether; copper(l) iodide; silver tetrafluoroborate; tert-butylhypochlorite; diethyl (2R,3R)-tartrate; 4 A molecular sieve; toluene-4-sulfonic acid; ozone; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; methanol; 2,2,4-trimethylpentane; dichloromethane; acetone;
DOI:10.1021/jo00002a008

Reference yield:

: 4435-54-5
2-Methylene-1-butanol

: 131703-72-5,131829-83-9
C₆₃H₇₈N₄O₁₂SSi

Guidance literature:: Multi-step reaction with 10 steps

1: L-(+)-diethyl tartrate, titanium(IV) isopropoxide, tert-butyl hydroperoxide, activated 4.0-Angstroem molecular sieves / CH₂Cl₂; 2,2,4-trimethyl-pentane / 1.) -20 deg C, 4 h, 2.) -15 deg C, 12 h

2: 91 percent / copper iodide / tetrahydrofuran / 1.) -25 to -30 deg C, 6 h, 2.) -15 deg C, 12 h

3: 99 percent / p-toluenesulfonic acid / acetone / 12 h

4: 1.) ozone, 2.) triphenylphosphine / 1.) CH₂Cl₂, -78 deg C, 15 min, 2.) room temperature, 24 h

6: 175 mg / 10percent aq. HCl / methanol / 0.25 h / Heating

7: triethylamine / CH₂Cl₂ / 26 h

8: N,N-diisopropylethylamine / tetrahydrofuran / 0.25 h / 0 °C

9: tert-butyl hypochlorite, triethylamine / CH₂Cl₂ / 0.08 h / 0 °C

10: HBF₄*Et₂O, AgBF₄ / acetone / 0.08 h

With titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; tetrafluoroboric acid diethyl ether; copper(l) iodide; silver tetrafluoroborate; tert-butylhypochlorite; diethyl (2R,3R)-tartrate; 4 A molecular sieve; toluene-4-sulfonic acid; ozone; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; methanol; 2,2,4-trimethylpentane; dichloromethane; acetone;
DOI:10.1021/jo00002a008

Reference yield:

: 4124-41-8
p-toluenesulfonylanhydride

: 131703-72-5,131829-83-9
C₆₃H₇₈N₄O₁₂SSi

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / CH₂Cl₂ / 24 h

2: triethylamine / tetrahydrofuran / 0.5 h / 0 °C

3: tert-butyl hypochlorite, triethylamine / CH₂Cl₂ / 0.08 h / 0 °C

4: HBF₄*Et₂O, AgBF₄ / acetone / 0.17 h

With tetrafluoroboric acid diethyl ether; silver tetrafluoroborate; tert-butylhypochlorite; triethylamine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/jo00002a008