6-benzamido-3-tert-butyl-3aα,5,6α,6aα-tetrahydro-4H-cyclopentisoxazole

Base Information

• Chemical Name: 6-benzamido-3-tert-butyl-3aα,5,6α,6aα-tetrahydro-4H-cyclopentisoxazole
• CAS No.: 127311-07-3
• Molecular Formula: C₁₇H₂₂N₂O₂
• Molecular Weight: 286.374

Synonyms:

Chemical Property of 6-benzamido-3-tert-butyl-3aα,5,6α,6aα-tetrahydro-4H-cyclopentisoxazole

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 6-benzamido-3-tert-butyl-3aα,5,6α,6aα-tetrahydro-4H-cyclopentisoxazole

There total 14 articles about 6-benzamido-3-tert-butyl-3aα,5,6α,6aα-tetrahydro-4H-cyclopentisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloro-2,2-dimethyl-propan-1-one oxime (3273-26-5) + N-(cyclopent-2-en-1-yl)-benzamide (3551-51-7) → 4-benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopentisoxazole (127311-17-5) + 6-benzamido-3-tert-butyl-3aα,5,6β,6aα-tetrahydro-4H-cyclopentisoxazole (127311-07-3,127380-39-6) + 6-benzamido-3-tert-butyl-3aα,5,6α,6aα-tetrahydro-4H-cyclopentisoxazole (127311-07-3,127380-39-6)

Guidance literature:

With triethylamine; In benzene; at 25 ℃; for 108h; Yield given. Yields of byproduct given;

Reference yield:

1-chloro-2,2-dimethyl-propan-1-one oxime (3273-26-5) + N-(cyclopent-2-en-1-yl)-benzamide (3551-51-7) → 4-benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopentisoxazole (127311-17-5) + 6-benzamido-3-tert-butyl-3aα,5,6β,6aα-tetrahydro-4H-cyclopentisoxazole (127311-07-3,127380-39-6) + 6-benzamido-3-tert-butyl-3aα,5,6α,6aα-tetrahydro-4H-cyclopentisoxazole (127311-07-3,127380-39-6)

Guidance literature:

With triethylamine; In benzene; at 25 ℃; for 108h; Yield given. Yields of byproduct given;

Reference yield:

N-(cyclopent-2-en-1-yl)-benzamide (3551-51-7) + tert-butyl nitrile oxide (27143-81-3) → 6-benzamido-3-tert-butyl-3aα,5,6α,6aα-tetrahydro-4H-cyclopentisoxazole (127311-07-3,127380-39-6)

Guidance literature:

In dichloromethane; at 25 ℃; for 108h;

DOI:10.1021/jo00299a004

upstream raw materials:

1-chloro-2,2-dimethyl-propan-1-one oxime

N-(cyclopent-2-en-1-yl)-benzamide

benzoyl chloride

tert-butyl nitrile oxide

Downstream raw materials:

6-(N-methyl)benzamido-3-tert-butyl-3aα,5,6β,6aα-tetrahydro-4H-cyclopentisoxazole

6-(N-methyl)benzamido-3-tert-butyl-3aα,5,6α,6aα-tetrahydro-4H-cyclopentisoxazole

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