2-cis-ethyl-5,6-cis-dimethyl-1,4-dithiocyclohexane

Base Information

• Chemical Name: 2-cis-ethyl-5,6-cis-dimethyl-1,4-dithiocyclohexane
• CAS No.: 122565-91-7
• Molecular Formula: C₈H₁₆S₂
• Molecular Weight: 176.347
• Mol file: 122565-91-7.mol

Synonyms:

Chemical Property of 2-cis-ethyl-5,6-cis-dimethyl-1,4-dithiocyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-cis-ethyl-5,6-cis-dimethyl-1,4-dithiocyclohexane

There total 2 articles about 2-cis-ethyl-5,6-cis-dimethyl-1,4-dithiocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) → Dibutyl sulfide (544-40-1) + 2,6-cis-3,5-trans-tetramethyl-1,4-dithiocyclohexane (122565-88-2) + 2-cis-ethyl-5,6-cis-dimethyl-1,4-dithiocyclohexane (122504-11-4,122565-91-7,122565-92-8,122565-93-9) + 2,6-cis-3,5-trans-tetramethyl-1,4-di(thioxo)cyclohexane (122504-14-7)

Guidance literature:

With carbon disulfide; carbon dioxide; ammonia; palladium(II) acetylacetonate; 1,2-bis-(diphenylphosphino)ethane; In N,N-dimethyl-formamide; at 150 ℃; for 20h; Further byproducts given. Title compound not separated from byproducts;

DOI:10.1007/BF00953627

Reference yield:

buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) → sec-butyl sulfide (626-26-6) + 2,6-cis-3,5-trans-tetramethyl-1,4-dithiocyclohexane (122565-88-2) + 2-cis-ethyl-5,6-cis-dimethyl-1,4-dithiocyclohexane (122504-11-4,122565-91-7,122565-92-8,122565-93-9) + 2,6-cis-3,5-trans-tetramethyl-1,4-di(thioxo)cyclohexane (122504-14-7)

Guidance literature:

With carbon disulfide; carbon dioxide; ammonia; palladium(II) acetylacetonate; 1,2-bis-(diphenylphosphino)ethane; In N,N-dimethyl-formamide; at 150 ℃; for 20h; Further byproducts given. Title compound not separated from byproducts;

DOI:10.1007/BF00953627

upstream raw materials:

buta-1,3-diene