Phosphoric acid, bis(1-methylethyl) 4-methyl-1-(1-methylethenyl)-6-(2,3,4,5-tetramethoxy-6-methylphenyl)-4- hexenyl ester, (E)-

Base Information

Chemical Name:Phosphoric acid, bis(1-methylethyl) 4-methyl-1-(1-methylethenyl)-6-(2,3,4,5-tetramethoxy-6-methylphenyl)-4- hexenyl ester, (E)-
CAS No.:139137-96-5
Molecular Formula:C27H45O8P
Molecular Weight:528.623
Hs Code.:

Synonyms:

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Chemical Property of Phosphoric acid, bis(1-methylethyl) 4-methyl-1-(1-methylethenyl)-6-(2,3,4,5-tetramethoxy-6-methylphenyl)-4- hexenyl ester, (E)-

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Technology Process of Phosphoric acid, bis(1-methylethyl) 4-methyl-1-(1-methylethenyl)-6-(2,3,4,5-tetramethoxy-6-methylphenyl)-4- hexenyl ester, (E)-

There total 3 articles about Phosphoric acid, bis(1-methylethyl) 4-methyl-1-(1-methylethenyl)-6-(2,3,4,5-tetramethoxy-6-methylphenyl)-4- hexenyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83036-57-1
(E)-1-(3,7-dimethylocta-2,6-dien-1-yl)-2,3,4,5-tetramethoxy-6-methylbenzene

: 139137-96-5
diisopropyl <(4E)-1-isopropenyl-4-methyl-6-(2,3,4,5-tetramethoxy-6-methylphenyl)-4-hexenyl>phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / mCPBA / CH₂Cl₂ / 1 h / 0 °C

2: (i-Pr)2NAlEt₂ / diethyl ether; hexane / 0.5 h / 0 °C

3: 1) BuLi / 1) THF, hexane, a) -78 deg C, 10 min, b) 0 deg C, 10 min, 2) 0 deg C, 15 min

With n-butyllithium; diisopropylamino diethylaluminium; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; hexane; dichloromethane;
DOI:10.1055/s-1991-28404

Reference yield:

: 85228-79-1
1-<(2E)-6,7-epoxy-3,7-dimethyloct-2-enyl>-2,3,4,5-tetramethoxy-6-methylbenzene

: 139137-96-5
diisopropyl <(4E)-1-isopropenyl-4-methyl-6-(2,3,4,5-tetramethoxy-6-methylphenyl)-4-hexenyl>phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: (i-Pr)2NAlEt₂ / diethyl ether; hexane / 0.5 h / 0 °C

2: 1) BuLi / 1) THF, hexane, a) -78 deg C, 10 min, b) 0 deg C, 10 min, 2) 0 deg C, 15 min

With n-butyllithium; diisopropylamino diethylaluminium; In diethyl ether; hexane;
DOI:10.1055/s-1991-28404

Reference yield:

: 2574-25-6
Diisopropyl chlorophosphate

: 85228-84-8
(E)-2,6-Dimethyl-8-(2,3,4,5-tetramethoxy-6-methyl-phenyl)-octa-1,6-dien-3-ol

: 139137-96-5
diisopropyl <(4E)-1-isopropenyl-4-methyl-6-(2,3,4,5-tetramethoxy-6-methylphenyl)-4-hexenyl>phosphate

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1) THF, hexane, a) -78 deg C, 10 min, b) 0 deg C, 10 min, 2) 0 deg C, 15 min;
DOI:10.1055/s-1991-28404