trans-9,10-dibenzoyloxy-1,2,3,6,7,8,9,10,11,12-decahydrobenzopyrene

Base Information

• Chemical Name: trans-9,10-dibenzoyloxy-1,2,3,6,7,8,9,10,11,12-decahydrobenzopyrene
• CAS No.: 68151-11-1
• Molecular Formula: C₃₄H₃₀O₄
• Molecular Weight: 502.61

Synonyms:

Chemical Property of trans-9,10-dibenzoyloxy-1,2,3,6,7,8,9,10,11,12-decahydrobenzopyrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-9,10-dibenzoyloxy-1,2,3,6,7,8,9,10,11,12-decahydrobenzopyrene

There total 1 articles about trans-9,10-dibenzoyloxy-1,2,3,6,7,8,9,10,11,12-decahydrobenzopyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2,3,6,7,8,9,10-Octahydrobenzopyrene (68151-10-0) + silver benzoate (532-31-0) → trans-9,10-dibenzoyloxy-1,2,3,6,7,8,9,10,11,12-decahydrobenzopyrene (68151-11-1)

Guidance literature:

With iodine; In benzene; Heating;

DOI:10.1021/jo01315a019

Reference yield:

trans-9,10-dibenzoyloxy-1,2,3,6,7,8,9,10,11,12-decahydrobenzopyrene (68151-11-1) → trans-9,10-Dihydroxy-9,10-dihydrobenzopyren (66788-06-5,88190-97-0)

Guidance literature:

Multi-step reaction with 4 steps

1: DDQ

2: NBS, (PhCO)2O₂

3: DBN

4: NaOMe

With N-Bromosuccinimide; 2,6-dichloro-benzonitrile; sodium methylate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; dibenzoyl peroxide;

DOI:10.1021/jo01315a019

Reference yield:

trans-9,10-dibenzoyloxy-1,2,3,6,7,8,9,10,11,12-decahydrobenzopyrene (68151-11-1) → C34H24O4

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone;

DOI:10.1021/jo01315a019

upstream raw materials:

1,2,3,6,7,8,9,10-Octahydrobenzopyrene

silver benzoate

Downstream raw materials:

trans-9,10-Dihydroxy-9,10-dihydrobenzopyren

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