dioxa-3,5 endo phenyl-4 anti tricyclo<5.2.1.0^2,6>decane

Base Information

• Chemical Name: dioxa-3,5 endo phenyl-4 anti tricyclo<5.2.1.0^2,6>decane
• CAS No.: 31112-51-3
• Molecular Formula: C₁₄H₁₆O₂
• Molecular Weight: 216.28

Synonyms:

Chemical Property of dioxa-3,5 endo phenyl-4 anti tricyclo<5.2.1.0^2,6>decane

Chemical Property:

Purity/Quality:

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Technology Process of dioxa-3,5 endo phenyl-4 anti tricyclo<5.2.1.0^2,6>decane

There total 1 articles about dioxa-3,5 endo phenyl-4 anti tricyclo<5.2.1.0^2,6>decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-endo,3-endo-bicyclo[2.2.1]heptane-2,3-diol (21462-06-6) + benzaldehyde (100-52-7) → dioxa-3,5 endo phenyl-4 anti tricyclo<5.2.1.02,6>decane (31112-51-3,31112-52-4,77341-47-0,77341-48-1)

Guidance literature:

With acide PTS; In benzene; for 0.666667h;

DOI:10.1016/0040-4020(80)80151-7

Reference yield: 90.7%

dioxa-3,5 endo phenyl-4 anti tricyclo<5.2.1.02,6>decane (31112-51-3,31112-52-4,77341-47-0,77341-48-1) → benzoyloxy-2 endo hydroxy-3 endo bicyclo <2.2.1> heptane (77085-41-7,77299-90-2) + bromo-2 exo hydroxy-3 endo bicyclo<2.2.1>heptane (77085-37-1,77341-49-2)

Guidance literature:

With N-Bromosuccinimide; In tetrachloromethane; for 3h; Heating;

DOI:10.1016/0040-4020(80)80151-7

upstream raw materials:

2-endo,3-endo-bicyclo[2.2.1]heptane-2,3-diol

benzaldehyde

Downstream raw materials:

benzoyloxy-2 endo hydroxy-3 endo bicyclo <2.2.1> heptane

bromo-2 exo hydroxy-3 endo bicyclo<2.2.1>heptane

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