Technology Process of 6-toluenesulfonylamino-6-deoxyfumagillol
There total 3 articles about 6-toluenesulfonylamino-6-deoxyfumagillol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 82 percent / CrO3*pyridine / CH2Cl2 / 1 h / Ambient temperature
2: 40 percent / NaBH3CN, AcONH4 / methanol / 1 h
3: aq. NaHCO3 / CHCl3 / 0.5 h
With
chromium trioxide-pyridine complex; ammonium acetate; sodium cyanoborohydride; sodium hydrogencarbonate;
In
methanol; dichloromethane; chloroform;
DOI:10.1248/cpb.40.575
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 40 percent / NaBH3CN, AcONH4 / methanol / 1 h
2: aq. NaHCO3 / CHCl3 / 0.5 h
With
ammonium acetate; sodium cyanoborohydride; sodium hydrogencarbonate;
In
methanol; chloroform;
DOI:10.1248/cpb.40.575
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
chloroform;
for 0.5h;
Yield given;
DOI:10.1248/cpb.40.575
