(6S,15RS)-11-deoxy-7,11-dioxa-PGI₁ methyl ester

Base Information

• Chemical Name: (6S,15RS)-11-deoxy-7,11-dioxa-PGI₁ methyl ester
• CAS No.: 90263-66-4
• Molecular Formula: C₁₉H₃₂O₆
• Molecular Weight: 356.459

Synonyms:

Chemical Property of (6S,15RS)-11-deoxy-7,11-dioxa-PGI₁ methyl ester

Chemical Property:

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Technology Process of (6S,15RS)-11-deoxy-7,11-dioxa-PGI₁ methyl ester

There total 1 articles about (6S,15RS)-11-deoxy-7,11-dioxa-PGI₁ methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 6,6-dimethoxyhexanoate (25176-55-0) → (6S,15RS)-11-deoxy-7,11-dioxa-PGI1 methyl ester (90263-66-4,90319-95-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 0.87 g / pyridinium tosylate / 1,2-dichloro-ethane / 6 h / Heating

2: 90 percent / oxalyl chloride, DMSO / CH₂Cl₂ / 0.33 h / -60 °C

3: 1.) sodium hydride / 1.) DME, RT, 1 h, 2.) 0 deg C (30 min), RT (2 h)

4: 73 percent / NaBH₄ / methanol / 0.5 h / -20 °C

With sodium tetrahydroborate; oxalyl dichloride; pyridinium p-toluenesulfonate; sodium hydride; dimethyl sulfoxide; In methanol; dichloromethane; 1,2-dichloro-ethane;

upstream raw materials:

methyl 6,6-dimethoxyhexanoate

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