rhizochalinin C perbenzoate

Base Information

• Chemical Name: rhizochalinin C perbenzoate
• CAS No.: 1003610-00-1
• Molecular Formula: C₆₃H₇₈N₂O₉
• Molecular Weight: 1007.32
• Mol file: 1003610-00-1.mol

Synonyms:

Chemical Property of rhizochalinin C perbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of rhizochalinin C perbenzoate

There total 3 articles about rhizochalinin C perbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

rhizochalin C (1004787-04-5) + benzoic acid (65-85-0,8013-63-6) → rhizochalinin C perbenzoate (1003610-00-1)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 144h;

DOI:10.1021/np0704811

Reference yield:

C51H76N2O8 → rhizochalinin C perbenzoate (1003610-00-1)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen; 2,2-dimethoxy-propane; hydrogenchloride / methanol / 10 h

2: pyridine

With pyridine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; 2,2-dimethoxy-propane; In methanol;

DOI:10.1021/jo302355t

Reference yield:

rhizochalinin C (1004787-15-8) + benzoyl chloride (98-88-4) → rhizochalinin C perbenzoate (1003610-00-1)

Guidance literature:

With pyridine;

DOI:10.1021/jo302355t

upstream raw materials:

rhizochalin C

benzoic acid

rhizochalinin C

benzoyl chloride