methyl 5β-hydroxy-3-oxocholan-24-oate

Base Information

Chemical Name:methyl 5β-hydroxy-3-oxocholan-24-oate
CAS No.:643758-93-4
Molecular Formula:C₂₅H₄₀O₄
Molecular Weight:404.59
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 5β-hydroxy-3-oxocholan-24-oate

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Technology Process of methyl 5β-hydroxy-3-oxocholan-24-oate

There total 2 articles about methyl 5β-hydroxy-3-oxocholan-24-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1173-32-6
methyl 3-oxo-5β-cholan-24-oate

: methyl 3,4-seco-5β-cholan-24-oate-3,4-dioic acid

: 1452-33-1
methyl 3-oxo-4-cholenolate

: 643758-93-4
methyl 5β-hydroxy-3-oxocholan-24-oate

Guidance literature:: With tert.-butylhydroperoxide; 4 A molecular sieve; 5,10,15,20-tetramesitylporphyrinato osmium(II) carbonyl; In benzene; Heating;
DOI:10.1021/jo061800g

Reference yield:

: 1173-32-6
methyl 3-oxo-5β-cholan-24-oate

: 1452-33-1
methyl 3-oxo-4-cholenolate

: 643758-93-4
methyl 5β-hydroxy-3-oxocholan-24-oate

: 643758-97-8
(20S)-3-oxo-5β-cholan-O-24,20-lactone

: (20S)-5β-hydroxy-3-oxocholan-O-24,20-lactone

Guidance literature:: With 2,6-dichloropyridine N-oxide; 4 A molecular sieve; hydrogen bromide; (carbonyl)(5,10,15,20-tetramesitylporphyrinato)ruthenium(II); In benzene; at 50 ℃; for 60h; Further Variations:; Reaction time; Product distribution;
DOI:10.1039/b314965j