C₂₂H₂₆NO₄⁽¹⁺⁾*C₆H₂N₃O₇^(1-)

Base Information

Chemical Name:C₂₂H₂₆NO₄⁽¹⁺⁾*C₆H₂N₃O₇^(1-)
CAS No.:78860-24-9
Molecular Formula:C₆H₂N₃O₇*C₂₂H₂₆NO₄
Molecular Weight:596.551
Hs Code.:

C<sub>22</sub>H<sub>26</sub>NO<sub>4</sub><sup>(1+)</sup>*C<sub>6</sub>H<sub>2</sub>N<sub>3</sub>O<sub>7</sub><sup>(1-)</sup>

Synonyms:

Suppliers and Price of C₂₂H₂₆NO₄⁽¹⁺⁾*C₆H₂N₃O₇^(1-)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₆NO₄⁽¹⁺⁾*C₆H₂N₃O₇^(1-)

Chemical Property:

Purity/Quality:

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Technology Process of C₂₂H₂₆NO₄⁽¹⁺⁾*C₆H₂N₃O₇^(1-)

There total 8 articles about C₂₂H₂₆NO₄⁽¹⁺⁾*C₆H₂N₃O₇^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90959-09-4
(E)-2,3-dihydro-3-(3',4'-dimethoxyphenylmethylene)-1H-isoindol-1-one

: 78860-24-9
C₂₂H₂₆NO₄⁽¹⁺⁾*C₆H₂N₃O₇^(1-)

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) 10M sodium hydroxide, 2.) hydrogen / Pd-C 10percent / 1.) ethanol, reflux, 1 h, 2.) room temperature

2: 10 g / polyphosphoric acid / 8 h / 70 °C

3: 11 g / toluene-p-sulphonic acid / toluene / 5 h / Heating

4: lithium aluminium hydride / tetrahydrofuran / 5 h / Heating

5: 6 g / acetone / 10 h / 0 °C

6: 0.9 g / aq. 33percent potassium hydroxide / H₂O / 3.5 h / Heating

7: IRA-400 activated resin / H₂O / run throuhg a column of resin

8: ethanol / Heating

With potassium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; PPA; IRA-400 activated resin; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; acetone; toluene;
DOI:10.1039/P19810001654

Reference yield:

: 78860-17-0
13,13a-dihydro-10,11-dimethoxyisoindolo<1,2-b><3>benzazepine-5,6(7H)-dione

: 78860-24-9
C₂₂H₂₆NO₄⁽¹⁺⁾*C₆H₂N₃O₇^(1-)

Guidance literature:: Multi-step reaction with 6 steps

1: 11 g / toluene-p-sulphonic acid / toluene / 5 h / Heating

2: lithium aluminium hydride / tetrahydrofuran / 5 h / Heating

3: 6 g / acetone / 10 h / 0 °C

4: 0.9 g / aq. 33percent potassium hydroxide / H₂O / 3.5 h / Heating

5: IRA-400 activated resin / H₂O / run throuhg a column of resin

6: ethanol / Heating

With potassium hydroxide; lithium aluminium tetrahydride; IRA-400 activated resin; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; water; acetone; toluene;
DOI:10.1039/P19810001654

Reference yield:

: 78860-14-7
3-(3,4-dimethoxybenzyl)phthalimidin-2-ylacetic acid

: 78860-24-9
C₂₂H₂₆NO₄⁽¹⁺⁾*C₆H₂N₃O₇^(1-)

Guidance literature:: Multi-step reaction with 7 steps

1: 10 g / polyphosphoric acid / 8 h / 70 °C

2: 11 g / toluene-p-sulphonic acid / toluene / 5 h / Heating

3: lithium aluminium hydride / tetrahydrofuran / 5 h / Heating

4: 6 g / acetone / 10 h / 0 °C

5: 0.9 g / aq. 33percent potassium hydroxide / H₂O / 3.5 h / Heating

6: IRA-400 activated resin / H₂O / run throuhg a column of resin

7: ethanol / Heating

With potassium hydroxide; lithium aluminium tetrahydride; PPA; IRA-400 activated resin; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; water; acetone; toluene;
DOI:10.1039/P19810001654