N-<3-<4--1-piperidinyl>propyl>-N-methylbenzeneamine

Base Information

Chemical Name:N-<3-<4--1-piperidinyl>propyl>-N-methylbenzeneamine
CAS No.:111951-91-8
Molecular Formula:C₂₈H₃₂F₂N₂
Molecular Weight:434.572
Hs Code.:

N-<3-<4-<bis(4-fluorophenyl)methyl>-1-piperidinyl>propyl>-N-methylbenzeneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<3-<4--1-piperidinyl>propyl>-N-methylbenzeneamine

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Technology Process of N-<3-<4--1-piperidinyl>propyl>-N-methylbenzeneamine

There total 4 articles about N-<3-<4--1-piperidinyl>propyl>-N-methylbenzeneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 111952-43-3
4--1-(3-chloropropyl)piperidine

: 100-61-8
N-methylaniline

: 111951-91-8
N-<3-<4--1-piperidinyl>propyl>-N-methylbenzeneamine

Guidance literature:: at 100 ℃; for 30h;
DOI:10.1021/jm00114a009

Reference yield:

: 60285-00-9
4-[bis(4-fluorophenyl)-methyl]piperidine

: 111951-91-8
N-<3-<4--1-piperidinyl>propyl>-N-methylbenzeneamine

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃ / butan-1-ol / 21 h / Heating

2: SOCl₂ / CHCl₃ / 6 h / Heating

3: 44 percent / 30 h / 100 °C

With thionyl chloride; sodium hydrogencarbonate; In chloroform; butan-1-ol;
DOI:10.1021/jm00114a009

Reference yield:

: 58113-36-3
4-(bis(4-fluorophenyl)methylene)piperidine

: 111951-91-8
N-<3-<4--1-piperidinyl>propyl>-N-methylbenzeneamine

Guidance literature:: Multi-step reaction with 4 steps

1: I₂, phosphorous, methanesulfonic acid / aq. acetic acid / 7 h / Heating

2: NaHCO₃ / butan-1-ol / 21 h / Heating

3: SOCl₂ / CHCl₃ / 6 h / Heating

4: 44 percent / 30 h / 100 °C

With phosphorus; thionyl chloride; methanesulfonic acid; iodine; sodium hydrogencarbonate; In chloroform; acetic acid; butan-1-ol;
DOI:10.1021/jm00114a009