5,10,15,20-tetra(o-tolyl)porphyrin iron(III) chloride

Base Information

• Chemical Name: 5,10,15,20-tetra(o-tolyl)porphyrin iron(III) chloride
• CAS No.: 86992-74-7
• Molecular Formula: C₄₈H₃₆ClFeN₄
• Molecular Weight: 760.141
• Mol file: 86992-74-7.mol

Synonyms:

Chemical Property of 5,10,15,20-tetra(o-tolyl)porphyrin iron(III) chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,10,15,20-tetra(o-tolyl)porphyrin iron(III) chloride

There total 2 articles about 5,10,15,20-tetra(o-tolyl)porphyrin iron(III) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.5%

5,10,15,20-tetrakis(o-methylphenyl)porphyrin (37083-40-2) → 5,10,15,20-tetra(o-tolyl)porphyrin iron(III) chloride (52155-50-7,86992-73-6,86992-74-7,86992-75-8,86992-76-9)

Guidance literature:

5,10,15,20-tetrakis(o-methylphenyl)porphyrin; With iron(II) chloride tetrahydrate; In N,N-dimethyl-formamide; for 0.5h;

With hydrogenchloride; In water; at 50 - 60 ℃;

DOI:10.3390/molecules16042960

Reference yield: 33.6%

pyrrole (109-97-7,30604-81-0) + 2-methylphenyl aldehyde (529-20-4) → 5,10,15,20-tetra(o-tolyl)porphyrin iron(III) chloride (52155-50-7,86992-73-6,86992-74-7,86992-75-8,86992-76-9)

Guidance literature:

pyrrole; 2-methylphenyl aldehyde; With acetic acid; propionic acid; In 1-methyl-3-nitrobenzene; for 0.416667h; Reflux;

With iron(II) chloride tetrahydrate; In 1-methyl-3-nitrobenzene; at 90 ℃; for 0.833333h; Reflux;

DOI:10.3390/molecules16042960

upstream raw materials:

pyrrole

2-methylphenyl aldehyde

5,10,15,20-tetrakis(o-methylphenyl)porphyrin