2-pentafluorophenylbutyric acid

Base Information

Chemical Name:2-pentafluorophenylbutyric acid
CAS No.:113423-80-6
Molecular Formula:C₁₀H₇F₅O₂
Molecular Weight:254.156
Hs Code.:

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Suppliers and Price of 2-pentafluorophenylbutyric acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-pentafluorophenylbutyric acid

Chemical Property:

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Technology Process of 2-pentafluorophenylbutyric acid

There total 3 articles about 2-pentafluorophenylbutyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 68598-72-1
ethyl 2-cyano-2-pentafluorophenylbutyrate

: 113423-80-6
2-pentafluorophenylbutyric acid

: 113423-81-7
ethyl-2-pentafluorophenylbutyrate

Guidance literature:: With sulfuric acid; In water; at 160 ℃; for 31h; Heating;
DOI:10.1039/P19870002129

Reference yield:

: 392-56-3
Hexafluorobenzene

: 113423-80-6
2-pentafluorophenylbutyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / K₂CO₃ / dimethylformamide / 5.5 h / 115 °C

2: 1.) NaH / 1.) DMF, 85 deg C, 17 h; 2.) 75 deg C, 24 h

3: 73 percent / conc. sulphuric acid / H₂O / 31 h / 160 °C / Heating

With sulfuric acid; sodium hydride; potassium carbonate; In water; N,N-dimethyl-formamide;
DOI:10.1039/P19870002129

Reference yield:

: 2340-87-6
ethyl α-cyanopentafluorophenylacetate

: 113423-80-6
2-pentafluorophenylbutyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 85 deg C, 17 h; 2.) 75 deg C, 24 h

2: 73 percent / conc. sulphuric acid / H₂O / 31 h / 160 °C / Heating

With sulfuric acid; sodium hydride; In water;
DOI:10.1039/P19870002129