3-deoxy-1,2-O-isopropylidene-3-bromo-4-fluoro-5-O-benzoyl-α-D-xylopentofuranose

Base Information

Chemical Name:3-deoxy-1,2-O-isopropylidene-3-bromo-4-fluoro-5-O-benzoyl-α-D-xylopentofuranose
CAS No.:111730-25-7
Molecular Formula:C₁₅H₁₆BrFO₅
Molecular Weight:375.191
Hs Code.:

Synonyms:

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Chemical Property of 3-deoxy-1,2-O-isopropylidene-3-bromo-4-fluoro-5-O-benzoyl-α-D-xylopentofuranose

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Technology Process of 3-deoxy-1,2-O-isopropylidene-3-bromo-4-fluoro-5-O-benzoyl-α-D-xylopentofuranose

There total 4 articles about 3-deoxy-1,2-O-isopropylidene-3-bromo-4-fluoro-5-O-benzoyl-α-D-xylopentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 94795-73-0
5-O-benzoyl-1,2-O-isopropylidene-3-deoxy-α-D-glycero-pent-3-enofuranose

: 111730-23-5
3-deoxy-1-fluoro-1,2-O-isopropylidene-3-bromo-5-O-benzoyl-D-threo(erythro)-pent-4-ulose

: 111730-25-7
3-deoxy-1,2-O-isopropylidene-3-bromo-4-fluoro-5-O-benzoyl-α-D-xylopentofuranose

Guidance literature:: With thallium(I) fluoride; bromine; In benzene;

Reference yield:

: 15919-16-1
5-β-formyl-4-β-O-tosyl-2α,3α-O-isopropylidenetetrahydrofuran

: 111730-25-7
3-deoxy-1,2-O-isopropylidene-3-bromo-4-fluoro-5-O-benzoyl-α-D-xylopentofuranose

Guidance literature:: Multi-step reaction with 4 steps

1: sodium acetate / acetonitrile / 0.25 h / Heating

2: NaBH₄ / methanol / 3 h / Ambient temperature

3: 89 percent / pyridine / 2 h / 5 °C

4: 11 percent / TlF, Br₂

With pyridine; sodium tetrahydroborate; thallium(I) fluoride; bromine; sodium acetate; In methanol; acetonitrile;

Reference yield:

: 14260-64-1
(3aR)-2,2-dimethyl-(3ar,6ac)-3a,6a-dihydro-furo[2,3-d][1,3]dioxole-5-carbaldehyde

: 111730-25-7
3-deoxy-1,2-O-isopropylidene-3-bromo-4-fluoro-5-O-benzoyl-α-D-xylopentofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / methanol / 3 h / Ambient temperature

2: 89 percent / pyridine / 2 h / 5 °C

3: 11 percent / TlF, Br₂

With pyridine; sodium tetrahydroborate; thallium(I) fluoride; bromine; In methanol;