Rh((C₆H₅)2P(CH₂)2SC₆H₅)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=Rh((C₆H₅)2P(CH₂)2SC₆H₅)2B(C₆H₅)4

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Chemical Name:Rh((C₆H₅)2P(CH₂)2SC₆H₅)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=Rh((C₆H₅)2P(CH₂)2SC₆H₅)2B(C₆H₅)4
CAS No.:87825-49-8
Molecular Formula:C₂₄H₂₀B*C₄₀H₃₈P₂RhS₂
Molecular Weight:1066.96
Hs Code.:

Rh((C<sub>6</sub>H<sub>5</sub>)2P(CH<sub>2</sub>)2SC<sub>6</sub>H<sub>5</sub>)2<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=Rh((C<sub>6</sub>H<sub>5</sub>)2P(CH<sub>2</sub>)2SC<sub>6</sub>H<sub>5</sub>)2B(C<sub>6</sub>H<sub>5</sub>)4

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Chemical Property of Rh((C₆H₅)2P(CH₂)2SC₆H₅)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=Rh((C₆H₅)2P(CH₂)2SC₆H₅)2B(C₆H₅)4

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Technology Process of Rh((C₆H₅)2P(CH₂)2SC₆H₅)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=Rh((C₆H₅)2P(CH₂)2SC₆H₅)2B(C₆H₅)4

There total 2 articles about Rh((C₆H₅)2P(CH₂)2SC₆H₅)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=Rh((C₆H₅)2P(CH₂)2SC₆H₅)2B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 19297-97-3
(2-(phenylthio)ethyl)diphenylphosphine

: 143-66-8
sodium tetraphenyl borate

: 87825-49-8,87859-26-5
{Rh((C₆H₅)2PCH₂CH₂SC₆H₅)2}⁽¹⁺⁾*{B(C₆H₅)4}^(1-)={Rh((C₆H₅)2PCH₂CH₂SC₆H₅)2}{B(C₆H₅)4}

Guidance literature:: In ethanol; mixt. of EtOH, ligand and Rh-complex was stirred (1 h) under N2, soln. of NaBPh4 in EtOH was added, stirred for 15 min; filtered, washed with EtOH, dried under vac.; elem. anal.;

Reference yield:

: (η(4)-cycloocta-1,5-diene)chlororhodium(I)

: 19297-97-3
(2-(phenylthio)ethyl)diphenylphosphine

: 143-66-8
sodium tetraphenyl borate

: 87825-49-8,87859-26-5
Rh((C₆H₅)2P(CH₂)2SC₆H₅)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=Rh((C₆H₅)2P(CH₂)2SC₆H₅)2B(C₆H₅)4

Guidance literature:: In methanol; under N2, mixt. of complex in CH3OH and ligand was refluxed, NaB(C6H5) in CH3OH was added to the cooled filtered soln.; recrystd. from CH2Cl2-CH3OH; elem. anal.;
DOI:10.1016/S0020-1693(00)82592-X

Reference yield: 80.0%

: 87825-49-8,87859-26-5
{Rh((C₆H₅)2PCH₂CH₂SC₆H₅)2}⁽¹⁺⁾*{B(C₆H₅)4}^(1-)={Rh((C₆H₅)2PCH₂CH₂SC₆H₅)2}{B(C₆H₅)4}

: 87825-51-2
RhCO((C₆H₅)2PCH₂CH₂SC₆H₅)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=RhCO((C₆H₅)2PCH₂CH₂SC₆H₅)2B(C₆H₅)4

Guidance literature:: With CO; In dichloromethane; Rh-complex was dissolved in CH2Cl2 under CO, EtOH was added, mixed; solvent was slowly evapd.; elem. anal.;