(Pt(P(C₆H₅)3)2(CS₃))

Base Information

Chemical Name:(Pt(P(C₆H₅)3)2(CS₃))
CAS No.:65354-15-6
Molecular Formula:C₃₇H₃₀P₂PtS₃
Molecular Weight:827.871
Hs Code.:

(Pt(P(C<sub>6</sub>H<sub>5</sub>)3)2(CS<sub>3</sub>))

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Chemical Property of (Pt(P(C₆H₅)3)2(CS₃))

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Technology Process of (Pt(P(C₆H₅)3)2(CS₃))

There total 4 articles about (Pt(P(C₆H₅)3)2(CS₃)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75-15-0,12122-00-8
carbon disulfide

: 76583-22-7,37580-97-5
cis-bis(thiolo)bis(triphenylphosphine)platinum(II)

: 65354-15-6
(Pt(P(C₆H₅)3)2(CS₃))

Guidance literature:: In carbon disulfide; CS2 added under N2 to solid Pt complex; stirred overnight; evapn.; recrystn. from CH2Cl2/hexane; elem. anal.;
DOI:10.1021/ic000825+

Reference yield: 70.0%

: 75-15-0,12122-00-8
carbon disulfide

: 10199-34-5,14056-88-3,15604-36-1
bis(triphenylphosphine)platinum(II) dichloride

: 65354-15-6
(Pt(P(C₆H₅)3)2(CS₃))

Guidance literature:: With NH₃; NH3 bubbled into CS2 cooled to -78°C until two distinct layers were formed, then added solid PtCl2(bis-phosphine) with stirring at -78°C for 2 h, slowly warmed to room temp. (excess of NH3 evapd.), residue placed under vac. for 1 h; extd. with CH2Cl2 ( 3 fold), vol. reduced, petroleum ether added with stirring, filtered, washed with MeOH and Et2O, dried overnight in vac., elem. anal.;
DOI:10.1016/S0277-5387(00)00295-3

Reference yield:

: [Pt2(CO)(PPh3)3(μ-S)]

: 65354-15-6
(Pt(P(C₆H₅)3)2(CS₃))

Guidance literature:: With CS₂; In carbon disulfide; Pt-complex was dissolved in CS2, filtered, pentane was added, chilled to -10°C; filtered, recrystd. from CH2Cl2/ethyl ether;