1-<3-propyl>-4-aminopiperidine

Base Information

Chemical Name:1-<3-propyl>-4-aminopiperidine
CAS No.:163981-89-3
Molecular Formula:C₁₉H₃₃N₃O₂
Molecular Weight:335.49
Hs Code.:

1-<3-<N-methyl-N-(3,4-dimethoxyphenethyl)amino>propyl>-4-aminopiperidine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<3-propyl>-4-aminopiperidine

Chemical Property:

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Technology Process of 1-<3-propyl>-4-aminopiperidine

There total 5 articles about 1-<3-propyl>-4-aminopiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1027036-42-5
1-(3-{[2-(3,4-Dimethoxy-phenyl)-ethyl]-methyl-amino}-propyl)-piperidin-4-one oxime

: 163981-89-3
1-<3-propyl>-4-aminopiperidine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 3h; Yield given; Heating;
DOI:10.1021/jm00013a017

Reference yield:

: 3490-06-0
N-methylhomoveratrylamine

: 163981-89-3
1-<3-propyl>-4-aminopiperidine

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

2: 1.) K₂CO₃, 2.) aq. HCl / 1.) methyl isopropyl ketone, reflux, overnight, 2.) reflux, 2 h

3: NH₂OH*HCl / ethanol; H₂O / 1 h / Heating

4: LiAlH₄ / tetrahydrofuran / 3 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; hydroxylamine hydrochloride; potassium carbonate; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00013a017

Reference yield:

: 36770-74-8
N-(3-chloropropyl)-3,4-dimethoxy-N-methylphenethylamine

: 163981-89-3
1-<3-propyl>-4-aminopiperidine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) K₂CO₃, 2.) aq. HCl / 1.) methyl isopropyl ketone, reflux, overnight, 2.) reflux, 2 h

2: NH₂OH*HCl / ethanol; H₂O / 1 h / Heating

3: LiAlH₄ / tetrahydrofuran / 3 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; hydroxylamine hydrochloride; potassium carbonate; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jm00013a017