SbCl(C₆H₅)(CH(Si(CH₃)3)2)

Base Information

Chemical Name:SbCl(C₆H₅)(CH(Si(CH₃)3)2)
CAS No.:911713-27-4
Molecular Formula:C₁₃H₂₄ClSbSi₂
Molecular Weight:393.708
Hs Code.:

SbCl(C<sub>6</sub>H<sub>5</sub>)(CH(Si(CH<sub>3</sub>)3)2)

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Chemical Property of SbCl(C₆H₅)(CH(Si(CH₃)3)2)

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Technology Process of SbCl(C₆H₅)(CH(Si(CH₃)3)2)

There total 1 articles about SbCl(C₆H₅)(CH(Si(CH₃)3)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.7%

: 86509-05-9
bis(trimethylsilyl)methylmagnesium chloride

: 5035-52-9
dichlorophenylstibine

: 911713-27-4
SbCl(C₆H₅)(CH(Si(CH₃)3)2)

Guidance literature:: In tetrahydrofuran; under Ar; (Me3Si)2CHMgCl (freshly prepd. from (Me3Si)2CHCl and Mg in THF) added dropwise to soln. of PhSbCl2 in THF under cooling with ice; mixt. refluxed for 1 h; stirred at room temp. for 20 h; evapd. under vac.; residue taken up in Et2O; Ar-satd. water added in ice-bath; org. phase sepd.; aq. phase extracted with Et2O; combined org. phases dried over Na2SO4; filtered; filtrate evapd.;
DOI:10.1515/znb-2005-1218

Reference yield: 64.0%

: 911713-27-4
SbCl(C₆H₅)(CH(Si(CH₃)3)2)

: 911713-26-3
(Sb(C₆H₅)(CH(Si(CH₃)3)2))2

Guidance literature:: With Mg; In tetrahydrofuran; under Ar; soln. of Ph((Me3Si)2CH)SbCl in THF added to Mg shavings activated with 1,2-dibromoethane in THF at -10°C; mixt. stirred at roomtemp. overnight; THF evapd. under vac.; residue taken up in petroleum ether; concd.; crystn. at -28°C;
DOI:10.1515/znb-2005-1218