1,3-bis(di(ortho-methoxyphenyl)phosphanyl)propane nickel(II) di(trifluoroacetate)

Base Information

• Chemical Name: 1,3-bis(di(ortho-methoxyphenyl)phosphanyl)propane nickel(II) di(trifluoroacetate)
• CAS No.: 353514-21-3
• Molecular Formula: C₃₅H₃₄F₆NiO₈P₂
• Molecular Weight: 817.278
• Mol file: 353514-21-3.mol

Synonyms:

Chemical Property of 1,3-bis(di(ortho-methoxyphenyl)phosphanyl)propane nickel(II) di(trifluoroacetate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1,3-bis(di(ortho-methoxyphenyl)phosphanyl)propane nickel(II) di(trifluoroacetate)

There total 1 articles about 1,3-bis(di(ortho-methoxyphenyl)phosphanyl)propane nickel(II) di(trifluoroacetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

nickel(II) acetate tetrahydrate (6018-89-9) + 1,3-bis[di(2-methoxyphenyl)-phosphino]propane (116163-96-3) + trifluoroacetic acid (76-05-1) → 1,3-bis(di(ortho-methoxyphenyl)phosphanyl)propane nickel(II) di(trifluoroacetate) (353514-21-3)

Guidance literature:

In methanol; dichloromethane; all manipulations under dry Ar or dry N2; Ni compd. dissolved in MeOH and mixed with soln. of ligand in CH2Cl2, addn. of soln. of CF3COOH; soln. filtered, filtrate layered with Et2O, ppt. collected; elem. anal.;

upstream raw materials:

nickel(II) acetate tetrahydrate

1,3-bis[di(2-methoxyphenyl)-phosphino]propane

trifluoroacetic acid