trans-2-(phenylseleno)-3-cyclohexanone

Base Information

• Chemical Name: trans-2-(phenylseleno)-3-cyclohexanone
• CAS No.: 107078-92-2
• Molecular Formula: C₂₂H₂₄N₂OSe
• Molecular Weight: 411.405
• Mol file: 107078-92-2.mol

Synonyms:

Chemical Property of trans-2-(phenylseleno)-3-cyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of trans-2-(phenylseleno)-3-cyclohexanone

There total 1 articles about trans-2-(phenylseleno)-3-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexenone (930-68-7) + Phenylselenyl bromide (34837-55-3) + 2-(N,N-dimethylamino)-2-phenylacetonitrile (827-36-1) → trans-2-(phenylseleno)-3-cyclohexanone (100514-93-0,107078-92-2)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/jo00358a024

Reference yield: 95.0%

trans-2-(phenylseleno)-3-cyclohexanone (100514-93-0,107078-92-2) → trans-2-(phenylseleno)-3-benzoylcyclohexanone (100514-95-2)

Guidance literature:

With silver nitrate; In tetrahydrofuran; diethyl ether; for 0.666667h; Ambient temperature;

DOI:10.1021/jo00358a024

upstream raw materials:

cyclohexenone

Phenylselenyl bromide

2-(N,N-dimethylamino)-2-phenylacetonitrile

Downstream raw materials:

trans-2-(phenylseleno)-3-benzoylcyclohexanone