Rh(Sb(C₆H₅)3)3COBr

Base Information

Chemical Name:Rh(Sb(C₆H₅)3)3COBr
CAS No.:47903-85-5
Molecular Formula:C₅₅H₄₅BrORhSb₃
Molecular Weight:1270.02
Hs Code.:

Rh(Sb(C<sub>6</sub>H<sub>5</sub>)3)3COBr

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Rh(Sb(C₆H₅)3)3COBr

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Technology Process of Rh(Sb(C₆H₅)3)3COBr

There total 1 articles about Rh(Sb(C₆H₅)3)3COBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39194-71-3
Rh(CO)Cl{Sb(C₆H₅)3}3

: 7550-35-8
lithium bromide

: 47903-85-5
Rh(Sb(C₆H₅)3)3COBr

Guidance literature:: In acetone; byproducts: LiCl; soln. of Rh-complex in acetone was treated with LiBr, refluxed for 45 min, cooled to room temp.; solvent was removed, extd. with benzene, filtered, evapd. to dryness, dried under reduced pressure for 2 ds;
DOI:10.1016/S0022-328X(01)00879-8

Reference yield: 64.0%

: 47903-85-5
Rh(Sb(C₆H₅)3)3COBr

: 56563-37-2
toluene-4-sulfonic acid but-2-ynyl ester

: 375387-35-2
Rh(SbPh3)3Br(η2-C(O)C(Me)=C(OTs)CH2)

Guidance literature:: In dichloromethane; soln. of Rh-complex in CH2Cl2 was treated with ligand at room temp., stirred for 1 h under Ar; vol. was reduced, hexane was added, filtered, washed with hexane, dried in vacuo;
DOI:10.1016/S0022-328X(01)00879-8